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Phosphocholine-Bonded Galactosylceramides Having a Tri-Unsaturated Long-Chain Base from the Clam Worm, Marphysa sanguinea

Seven glycosphingolipids were obtained in the pure state from the clam worm, Marphysa sanguinea, by preparative HPLC with a reversed-phase column in a recycling mode. Their structures were elucidated based on detailed analyses of iH- and 13C-NMR spectra of the intact compounds. The position and the...

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Published in:	Journal of biochemistry (Tokyo) 1994-08, Vol.116 (2), p.435-442
Main Authors:	Noda, Naoki, Tanaka, Ryuichiro, Tsujino, Kazushige, Takasaki, Yoko, Nakano, Masami, Nishi, Masatoshi, Miyahara, Kazumoto
Format:	Article
Language:	English
Subjects:	Animals Annelida - chemistry Chromatography, High Pressure Liquid Galactosylceramides - chemistry Galactosylceramides - isolation & purification glycosphingolipid Magnetic Resonance Spectroscopy - methods Marine Marphysa sanguinea Molecular Conformation phosphocholine-galactosylcer-amide Phosphorylcholine - chemistry Phosphorylcholine - isolation & purification Polychaeta recycling HPLC tri-unsaturated long-chain base
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cited_by	cdi_FETCH-LOGICAL-c528t-6ec2ed46c32f1f073687a1575243b8b60e0c8dd783f04b457605e01dfdc6baec3
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container_issue	2
container_start_page	435
container_title	Journal of biochemistry (Tokyo)
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creator	Noda, Naoki Tanaka, Ryuichiro Tsujino, Kazushige Takasaki, Yoko Nakano, Masami Nishi, Masatoshi Miyahara, Kazumoto
description	Seven glycosphingolipids were obtained in the pure state from the clam worm, Marphysa sanguinea, by preparative HPLC with a reversed-phase column in a recycling mode. Their structures were elucidated based on detailed analyses of iH- and 13C-NMR spectra of the intact compounds. The position and the geometry of double bonds in the long-chain base (LCB) were determined by the two-dimensional NMR (COSY, NOESY, and HMBC) analyses. All compounds are phosphocholine-bonded monogalactosylceramides and two of them have tri-unsaturated long-chain bases.
doi_str_mv	10.1093/oxfordjournals.jbchem.a124543
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source	J-STAGE (Japan Science & Technology Information Aggregator, Electronic) - Open Access English articles; Oxford University Press Archive
subjects	Animals Annelida - chemistry Chromatography, High Pressure Liquid Galactosylceramides - chemistry Galactosylceramides - isolation & purification glycosphingolipid Magnetic Resonance Spectroscopy - methods Marine Marphysa sanguinea Molecular Conformation phosphocholine-galactosylcer-amide Phosphorylcholine - chemistry Phosphorylcholine - isolation & purification Polychaeta recycling HPLC tri-unsaturated long-chain base
title	Phosphocholine-Bonded Galactosylceramides Having a Tri-Unsaturated Long-Chain Base from the Clam Worm, Marphysa sanguinea
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