GLC Determination of 1-(2,6-dimethylphenoxy)-2-aminopropane in Urine

A rapid, sensitive, and accurate GLC method of analysis of a new anticonvulsant drug, 1-(2,6-dimethylphenoxy)-2-aminopropane, was developed, utilizing an acid hydrolysis procedure to increase its degree of recovery from urine and employing one of its isomers, 1-(2,3-dimethylphenoxy)-2-aminopropane,...

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Bibliographic Details
Published in:Journal of pharmaceutical sciences 1973-08, Vol.62 (8), p.1376-1378
Main Authors: Szinai, Naomi, Perchalski, Robert J., Hammer, Richard H., Wilder, B.Joe, Streiff, Richard R.
Format: Article
Language:English
Subjects:
1-(2,6-Dimethylphenoxy)-2-aminopropane—GLC analysis in urine
6-dimethylphenoxy)-2-aminopropane in urine
6-Dimethylphenoxy)-2-aminopropane-GLC analysis in urine
Amphetamine - urine
Anticonvulsants - urine
Chromatography, Gas
GLC-analysis
GLC—analysis, 1-(2,6-dimethylphenoxy)-2-aminopropane in urine
Humans
Hydrolysis
Methods
Phenols - urine
Propane - urine
Propylamines - urine
Solvents
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Summary:A rapid, sensitive, and accurate GLC method of analysis of a new anticonvulsant drug, 1-(2,6-dimethylphenoxy)-2-aminopropane, was developed, utilizing an acid hydrolysis procedure to increase its degree of recovery from urine and employing one of its isomers, 1-(2,3-dimethylphenoxy)-2-aminopropane, as an internal standard.
ISSN:0022-3549
1520-6017
DOI:10.1002/jps.2600620840