XRD and IR analysis of nanocrystalline Ni–Zn ferrite synthesized by the sol–gel method

Nanocrystalline Ni 1− x Zn x Fe 2O 4 ( x = 0.0, 0.2, 0.4, 0.6, 0.8, and 1.0) ferrites were synthesized by the sol–gel method. The obtained powder was annealed at temperatures from 500 to 1000 °C. X-ray diffraction (XRD) and infrared spectroscopy (IR) were used to study the structural changes taking...

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Bibliographic Details
Published in:Materials letters 2011-02, Vol.65 (4), p.677-680
Main Authors: Raghavender, A.T., Biliškov, N., Skoko, Ž.
Format: Article
Language:English
Subjects:
Diffraction
Ferrite
Grain size
Infrared radiation
Infrared spectroscopy
Nanocrystals
Nanomaterials
Ni–Zn ferrite
Sol gel process
Structural properties
temperature
X-ray diffraction
Zinc
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Summary:Nanocrystalline Ni 1− x Zn x Fe 2O 4 ( x = 0.0, 0.2, 0.4, 0.6, 0.8, and 1.0) ferrites were synthesized by the sol–gel method. The obtained powder was annealed at temperatures from 500 to 1000 °C. X-ray diffraction (XRD) and infrared spectroscopy (IR) were used to study the structural changes taking place with varying Zn content x. The grain size decreased while the lattice parameter increases with the increase of the Zn content.
ISSN:0167-577X
1873-4979
DOI:10.1016/j.matlet.2010.11.071