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Parameter Validation of Analytical Methods of Insecticide Residue Analyses in Foods of Animal Origin, Feed and Water
The study was conducted to examine the interrelationship and coherence of analytical parameters in method validation. Recovery, sensitivity, linearity, precision and limits of detection (LOD) were tested in six methods for organochlorine and organophosphate insecticides. Compounds that fell out of t...
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| Published in: | Bulletin of environmental contamination and toxicology 2011-06, Vol.86 (6), p.571-575 |
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| Main Authors: | , |
| Format: | Article |
| Language: | English |
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| cited_by | cdi_FETCH-LOGICAL-c402t-cef16cd3a2443ff34cc8ee4b5ba107bc1ea4aaed07db098e65788492dfecc1c53 |
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| cites | cdi_FETCH-LOGICAL-c402t-cef16cd3a2443ff34cc8ee4b5ba107bc1ea4aaed07db098e65788492dfecc1c53 |
| container_end_page | 575 |
| container_issue | 6 |
| container_start_page | 571 |
| container_title | Bulletin of environmental contamination and toxicology |
| container_volume | 86 |
| creator | Debebe, Amsalu Kuttalam, S. |
| description | The study was conducted to examine the interrelationship and coherence of analytical parameters in method validation. Recovery, sensitivity, linearity, precision and limits of detection (LOD) were tested in six methods for organochlorine and organophosphate insecticides. Compounds that fell out of the stipulated recovery, 70–120%, in a matrix have concurrently failed to meet the requirements for sensitivity (≥0.7), linearity (R
2
> 0.99) and precision ( |
| doi_str_mv | 10.1007/s00128-011-0284-1 |
| format | article |
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2
> 0.99) and precision (<0.2) in the same matrix. Highest LOD was recorded in those compounds and matrices. 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| fulltext | fulltext |
| identifier | ISSN: 0007-4861 |
| ispartof | Bulletin of environmental contamination and toxicology, 2011-06, Vol.86 (6), p.571-575 |
| issn | 0007-4861 1432-0800 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_876224972 |
| source | Springer Nature |
| subjects | Animal Feed - analysis Animals Aquatic Pollution Earth and Environmental Science Ecotoxicology Environment Environmental Chemistry Environmental Health Environmental Monitoring - methods Environmental Monitoring - standards Environmental Pollutants - analysis Feeds Food Analysis - methods Food Analysis - standards Food contamination & poisoning Food Contamination - analysis Food Contamination - statistics & numerical data Food Safety Fresh Water - chemistry Insecticides Insecticides - analysis Limit of Detection Organic compounds Organophosphates Parameter identification Pesticide Residues - analysis Pollution Soil Science & Conservation Waste Water Technology Water Management Water Pollution Control |
| title | Parameter Validation of Analytical Methods of Insecticide Residue Analyses in Foods of Animal Origin, Feed and Water |
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