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Investigations on the growth and characterization of l-citrulline oxalate monohydrate single crystal
New single crystals of l-citrulline oxalate (LCO) monohydrate are grown from aqueous solution by slow evaporation technique. Structure and morphology of the grown crystals are identified by single crystal XRD. The compound crystallizes in the orthorhombic structure with space group P2 12 12 1, havin...
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| Published in: | Journal of crystal growth 2011-06, Vol.324 (1), p.172-176 |
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| Main Authors: | , |
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| Language: | English |
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| cites | cdi_FETCH-LOGICAL-c374t-787fd3901d03a83753fa0a239969534147c15fd502f9681142f989f608871a113 |
| container_end_page | 176 |
| container_issue | 1 |
| container_start_page | 172 |
| container_title | Journal of crystal growth |
| container_volume | 324 |
| creator | Sreevalsa, V.G. Jayalekshmi, S. |
| description | New single crystals of
l-citrulline oxalate (LCO) monohydrate are grown from aqueous solution by slow evaporation technique. Structure and morphology of the grown crystals are identified by single crystal XRD. The compound crystallizes in the orthorhombic structure with space group P2
12
12
1, having cell parameters,
a=5.208(5)
Å,
b=9.829(5)
Å and
c=23.879(5)
Å. Powder X-ray diffraction data is used for the assignment of the hkl values. The chemical composition of the synthesized crystals is verified by CHN analysis. Functional groups present in the sample are identified by Fourier transform infra red (FT-IR) and FT-Raman spectral analysis. The second harmonic signal generated by the crystal using pulsed Nd: YAG Laser is confirmed by the emission of green radiation, showing that the crystal is a potential candidate for nonlinear optical studies. |
| doi_str_mv | 10.1016/j.jcrysgro.2011.03.017 |
| format | article |
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l-citrulline oxalate (LCO) monohydrate are grown from aqueous solution by slow evaporation technique. Structure and morphology of the grown crystals are identified by single crystal XRD. The compound crystallizes in the orthorhombic structure with space group P2
12
12
1, having cell parameters,
a=5.208(5)
Å,
b=9.829(5)
Å and
c=23.879(5)
Å. Powder X-ray diffraction data is used for the assignment of the hkl values. The chemical composition of the synthesized crystals is verified by CHN analysis. Functional groups present in the sample are identified by Fourier transform infra red (FT-IR) and FT-Raman spectral analysis. The second harmonic signal generated by the crystal using pulsed Nd: YAG Laser is confirmed by the emission of green radiation, showing that the crystal is a potential candidate for nonlinear optical studies.</description><identifier>ISSN: 0022-0248</identifier><identifier>EISSN: 1873-5002</identifier><identifier>DOI: 10.1016/j.jcrysgro.2011.03.017</identifier><identifier>CODEN: JCRGAE</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>A1. Crystal structure ; A1. Recrystallization ; A1. X-ray diffraction ; A2. Growth from solutions ; A2. Single crystal growth ; B1. Organic compounds ; Condensed matter: electronic structure, electrical, magnetic, and optical properties ; Condensed matter: structure, mechanical and thermal properties ; Cross-disciplinary physics: materials science; rheology ; Crystals ; Diffraction ; Emission analysis ; Exact sciences and technology ; Growth from solutions ; Harmonics ; Materials science ; Methods of crystal growth; physics of crystal growth ; Morphology ; Nonlinearity ; Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation ; Optical properties of bulk materials and thin films ; Oxalates ; Physics ; Single crystals ; Structure of solids and liquids; crystallography ; Structure of specific crystalline solids ; Theory and models of crystal growth; physics of crystal growth, crystal morphology and orientation</subject><ispartof>Journal of crystal growth, 2011-06, Vol.324 (1), p.172-176</ispartof><rights>2011 Elsevier B.V.</rights><rights>2015 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c374t-787fd3901d03a83753fa0a239969534147c15fd502f9681142f989f608871a113</citedby><cites>FETCH-LOGICAL-c374t-787fd3901d03a83753fa0a239969534147c15fd502f9681142f989f608871a113</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27901,27902</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=24276896$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Sreevalsa, V.G.</creatorcontrib><creatorcontrib>Jayalekshmi, S.</creatorcontrib><title>Investigations on the growth and characterization of l-citrulline oxalate monohydrate single crystal</title><title>Journal of crystal growth</title><description>New single crystals of
l-citrulline oxalate (LCO) monohydrate are grown from aqueous solution by slow evaporation technique. Structure and morphology of the grown crystals are identified by single crystal XRD. The compound crystallizes in the orthorhombic structure with space group P2
12
12
1, having cell parameters,
a=5.208(5)
Å,
b=9.829(5)
Å and
c=23.879(5)
Å. Powder X-ray diffraction data is used for the assignment of the hkl values. The chemical composition of the synthesized crystals is verified by CHN analysis. Functional groups present in the sample are identified by Fourier transform infra red (FT-IR) and FT-Raman spectral analysis. The second harmonic signal generated by the crystal using pulsed Nd: YAG Laser is confirmed by the emission of green radiation, showing that the crystal is a potential candidate for nonlinear optical studies.</description><subject>A1. Crystal structure</subject><subject>A1. Recrystallization</subject><subject>A1. X-ray diffraction</subject><subject>A2. Growth from solutions</subject><subject>A2. Single crystal growth</subject><subject>B1. Organic compounds</subject><subject>Condensed matter: electronic structure, electrical, magnetic, and optical properties</subject><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Crystals</subject><subject>Diffraction</subject><subject>Emission analysis</subject><subject>Exact sciences and technology</subject><subject>Growth from solutions</subject><subject>Harmonics</subject><subject>Materials science</subject><subject>Methods of crystal growth; physics of crystal growth</subject><subject>Morphology</subject><subject>Nonlinearity</subject><subject>Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation</subject><subject>Optical properties of bulk materials and thin films</subject><subject>Oxalates</subject><subject>Physics</subject><subject>Single crystals</subject><subject>Structure of solids and liquids; crystallography</subject><subject>Structure of specific crystalline solids</subject><subject>Theory and models of crystal growth; physics of crystal growth, crystal morphology and orientation</subject><issn>0022-0248</issn><issn>1873-5002</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><recordid>eNqFUEFuFDEQtBCRWAJfQL5EnGbotmfGnltQRCBSJC5wtiyPveuV1w62N7C8Ph42cOXS1Yeqrq4i5B1Cj4DTh32_N_lUtjn1DBB74D2geEE2KAXvRgD2kmzaZB2wQb4ir0vZAzQlwoYsd_HRluq3uvoUC02R1p2l7djPuqM6LtTsdNam2ux__-HQ5GjojK_5GIKPlqZfOuhq6SHFtDsted2Lj9tg6fpX1eENuXA6FPv2GS_J99tP326-dPdfP9_dfLzvDBdD7YQUbuEz4AJcSy5G7jRoxud5mkc-4CAMjm4Zgbl5kohDQzm7CaQUqBH5JXl_vvuQ049ji6UOvhgbgo42HYuSch4Y4-PUmNOZaXIqJVunHrI_6HxSCGptVe3V31bV2qoCrlqrTXj1bKGL0cFlHY0v_9RsYGKS82pwfebZlvfR26yK8TYau_hsTVVL8v-zegI_q5Hf</recordid><startdate>20110601</startdate><enddate>20110601</enddate><creator>Sreevalsa, V.G.</creator><creator>Jayalekshmi, S.</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20110601</creationdate><title>Investigations on the growth and characterization of l-citrulline oxalate monohydrate single crystal</title><author>Sreevalsa, V.G. ; Jayalekshmi, S.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c374t-787fd3901d03a83753fa0a239969534147c15fd502f9681142f989f608871a113</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>A1. Crystal structure</topic><topic>A1. Recrystallization</topic><topic>A1. X-ray diffraction</topic><topic>A2. Growth from solutions</topic><topic>A2. Single crystal growth</topic><topic>B1. Organic compounds</topic><topic>Condensed matter: electronic structure, electrical, magnetic, and optical properties</topic><topic>Condensed matter: structure, mechanical and thermal properties</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>Crystals</topic><topic>Diffraction</topic><topic>Emission analysis</topic><topic>Exact sciences and technology</topic><topic>Growth from solutions</topic><topic>Harmonics</topic><topic>Materials science</topic><topic>Methods of crystal growth; physics of crystal growth</topic><topic>Morphology</topic><topic>Nonlinearity</topic><topic>Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation</topic><topic>Optical properties of bulk materials and thin films</topic><topic>Oxalates</topic><topic>Physics</topic><topic>Single crystals</topic><topic>Structure of solids and liquids; crystallography</topic><topic>Structure of specific crystalline solids</topic><topic>Theory and models of crystal growth; physics of crystal growth, crystal morphology and orientation</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Sreevalsa, V.G.</creatorcontrib><creatorcontrib>Jayalekshmi, S.</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of crystal growth</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Sreevalsa, V.G.</au><au>Jayalekshmi, S.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Investigations on the growth and characterization of l-citrulline oxalate monohydrate single crystal</atitle><jtitle>Journal of crystal growth</jtitle><date>2011-06-01</date><risdate>2011</risdate><volume>324</volume><issue>1</issue><spage>172</spage><epage>176</epage><pages>172-176</pages><issn>0022-0248</issn><eissn>1873-5002</eissn><coden>JCRGAE</coden><abstract>New single crystals of
l-citrulline oxalate (LCO) monohydrate are grown from aqueous solution by slow evaporation technique. Structure and morphology of the grown crystals are identified by single crystal XRD. The compound crystallizes in the orthorhombic structure with space group P2
12
12
1, having cell parameters,
a=5.208(5)
Å,
b=9.829(5)
Å and
c=23.879(5)
Å. Powder X-ray diffraction data is used for the assignment of the hkl values. The chemical composition of the synthesized crystals is verified by CHN analysis. Functional groups present in the sample are identified by Fourier transform infra red (FT-IR) and FT-Raman spectral analysis. The second harmonic signal generated by the crystal using pulsed Nd: YAG Laser is confirmed by the emission of green radiation, showing that the crystal is a potential candidate for nonlinear optical studies.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/j.jcrysgro.2011.03.017</doi><tpages>5</tpages></addata></record> |
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| ispartof | Journal of crystal growth, 2011-06, Vol.324 (1), p.172-176 |
| issn | 0022-0248 1873-5002 |
| language | eng |
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| source | ScienceDirect Freedom Collection |
| subjects | A1. Crystal structure A1. Recrystallization A1. X-ray diffraction A2. Growth from solutions A2. Single crystal growth B1. Organic compounds Condensed matter: electronic structure, electrical, magnetic, and optical properties Condensed matter: structure, mechanical and thermal properties Cross-disciplinary physics: materials science rheology Crystals Diffraction Emission analysis Exact sciences and technology Growth from solutions Harmonics Materials science Methods of crystal growth physics of crystal growth Morphology Nonlinearity Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation Optical properties of bulk materials and thin films Oxalates Physics Single crystals Structure of solids and liquids crystallography Structure of specific crystalline solids Theory and models of crystal growth physics of crystal growth, crystal morphology and orientation |
| title | Investigations on the growth and characterization of l-citrulline oxalate monohydrate single crystal |
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