Preparation of YSZ coatings by thermal pressure and filtration of sol–gel paint (TPFSP) for thermal barrier application

• Published in: Surface & coatings technology 2011-06, Vol.205 (19), p.4343-4348
• Main Authors: Zhang, K., Ren, C., He, Y.D., Gao, W.
• Format: Article
• Language: English
• Subjects: Applied sciences; Coatings; Composite sol–gel coating; Corrosion; Corrosion environments; Cross-disciplinary physics: materials science; rheology; Cyclic oxidation resistance; Exact sciences and technology; Materials science; Metals. Metallurgy; Nanostructure; Nonmetallic coatings; Paints; Physics; Production techniques; Protective coatings; Sol gel process; Surface treatment; Surface treatments; Thermal barrier effect; Thermal pressure; Yttria stabilized zirconia; Yttria stabilized zirconia (YSZ); Zirconium
• ISSN: 0257-8972; 1879-3347
• DOI: 10.1016/j.surfcoat.2011.02.033

Thick YSZ ceramic coatings were prepared by thermal pressure and filtration of sol–gel paint (TPFSP), a modified sol–gel composite coating technique. SEM results show that the coatings were dense and crack-free by using paints of high mass ratios of YSZ powder to Zr–Y oxide in sol and high pressures. And the cross-sectional detail of coatings exhibited that the microstructure was consisted of micro/nano-size ceramic particles and micro-pores. The thermal insulation tests indicated that mass ratio of YSZ powder to Zr–Y oxide in sol was in inversely linear relationship with temperature drop per micron thickness. The coating showed good adherence with alloy substrate and maintained structural integrity when exposed at 1050°C for 200h. The cyclic oxidation test also indicated that both of oxidation resistance and spallation resistance for YSZ coated specimens were greatly improved. The TPFSP process could be a promising method to prepare TBCs for wide applications. ► Thick YSZ ceramic coatings were prepared by thermal pressure and filtration of sol–gel paint (TPFSP), a modified sol–gel composite coating technique. ► The influences of mass ratios of YSZ powder to Zr–Y oxides in sol and external pressure on the microstructure and thermal insulation performance were studied by a home-made measuring method. ► The cyclic oxidation tests indicate that both of oxidation resistance and spallation resistance of YSZ coatings were greatly improved. ► The TPFSP process could be a promising method to prepare TBCs for wide applications.