Synthesis, characterization and antifungal studies of arylspiroborates derived from 4-nitrocatechol

► Arylspiroborates are presented. ► Reactions with boric acid, 4-nitrocatechol and hydroxides. ► Antifungal studies preformed. ► Boron based wood preservatives. A family of arylspiroborates has been prepared by the addition of 4-nitrocatechol, boric acid and either an alkali metal hydroxide or an am...

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Bibliographic Details
Published in:Journal of molecular structure 2011-09, Vol.1002 (1), p.24-27
Main Authors: Mosseler, Joseph A., Melanson, Jennifer A., Bowes, Eric G., Lee, Graham M., Vogels, Christopher M., Baerlocher, Felix J., Decken, Andreas, Westcott, Stephen A.
Format: Article
Language:English
Subjects:
ammonium hydroxide
antifungal properties
Antifungal studies
Arylspiroborates
boric acid
Boron
nuclear magnetic resonance spectroscopy
X-ray diffraction
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Summary:► Arylspiroborates are presented. ► Reactions with boric acid, 4-nitrocatechol and hydroxides. ► Antifungal studies preformed. ► Boron based wood preservatives. A family of arylspiroborates has been prepared by the addition of 4-nitrocatechol, boric acid and either an alkali metal hydroxide or an ammonium hydroxide. All compounds were characterized fully using multinuclear NMR spectroscopy, FT-IR spectroscopy and by elemental analyses. A single crystal X-ray diffraction was carried out on triethylmethylammonium 4-nitro[1,2-benzenediolato(2-)-O,O′]borate ( 5). All new compounds were tested for potential fungicidal activity.
ISSN:0022-2860
1872-8014
DOI:10.1016/j.molstruc.2011.06.034