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Nonenzymatic glucose sensor based on renewable electrospun Ni nanoparticle-loaded carbon nanofiber paste electrode

A novel nonenzymatic glucose sensor was developed based on the renewable Ni nanoparticle-loaded carbon nanofiber paste (NiCFP) electrode. The NiCF nanocomposite was prepared by combination of electrospinning technique with thermal treatment method. The scanning electron microscopy (SEM) and transmis...

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Published in:Biosensors & bioelectronics 2009-07, Vol.24 (11), p.3329-3334
Main Authors: Liu, Yang, Teng, Hong, Hou, Haoqing, You, Tianyan
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description A novel nonenzymatic glucose sensor was developed based on the renewable Ni nanoparticle-loaded carbon nanofiber paste (NiCFP) electrode. The NiCF nanocomposite was prepared by combination of electrospinning technique with thermal treatment method. The scanning electron microscopy (SEM) and transmission electron microscopy (TEM) images showed that large amounts of spherical nanoparticles were well dispersed on the surface or embedded in the carbon nanofibers. And the nanoparticles were composed of Ni and NiO, as revealed by energy dispersive X-ray spectroscopy (EDX) and X-ray powder diffraction (XRD). In application to nonenzymatic glucose determination, the renewable NiCFP electrodes, which were constructed by simply mixing the electrospun nanocomposite with mineral oil, exhibited strong and fast amperometric response without being poisoned by chloride ions. Low detection limit of 1 μM with wide linear range from 2 μM to 2.5 mM ( R = 0.9997) could be obtained. The current response of the proposed glucose sensor was highly sensitive and stable, attributing to the electrocatalytic performance of the firmly embedded Ni nanoparticles as well as the chemical inertness of the carbon-based electrode. The good analytical performance, low cost and straightforward preparation method made this novel electrode material promising for the development of effective glucose sensor.
doi_str_mv 10.1016/j.bios.2009.04.032
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subjects Biological and medical sciences
Biosensing Techniques - instrumentation
Biotechnology
Carbon - chemistry
Electrochemistry - instrumentation
Electrochemistry - methods
Electrospinning
Equipment Design
Equipment Failure Analysis
Equipment Reuse
Fundamental and applied biological sciences. Psychology
Glucose
Glucose - analysis
Glucose - chemistry
Microelectrodes
Nanoparticles - chemistry
Nanoparticles - ultrastructure
Ni nanoparticle-loaded carbon nanofiber
Nickel - chemistry
Nonenzymatic sensor
Ointments - chemistry
Renewable electrode
Rotation
Transducers
title Nonenzymatic glucose sensor based on renewable electrospun Ni nanoparticle-loaded carbon nanofiber paste electrode
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