Laser ablation fast pulse discharge plasma spectroscopy analysis of Pb, Mg and Sn in soil

Laser ablation fast pulse discharge plasma spectroscopy (LA-FPDPS) technique is a recently developed atomic emission analytical technique that is analogous to dual pulse laser induced breakdown spectroscopy (DP-LIBS). LA-FPDPS, however, uses a periodical oscillating discharge plasma generation metho...

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Published in:Optics communications 2012, Vol.285 (1), p.54-58
Main Authors: Li, Xiafen, Zhou, Weidong, Li, Kexue, Qian, Huiguo, Ren, Zhijun
Format: Article
Language:English
Subjects:
Deposition
Electric discharges
Fast pulse discharge plasma
Laser ablation
Lead (metal)
LIBS
Magnesium
Soil (material)
Soil analysis
Spectroscopy
Tin
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description Laser ablation fast pulse discharge plasma spectroscopy (LA-FPDPS) technique is a recently developed atomic emission analytical technique that is analogous to dual pulse laser induced breakdown spectroscopy (DP-LIBS). LA-FPDPS, however, uses a periodical oscillating discharge plasma generation method on samples instead of the second laser beam in DP-LIBS. Here we describe the electric characteristics and its application to the analysis of Pb, Mg and Sn in soil. Due to the fast discharge process, the peak power deposition rate is up to 1.5 MW, although the discharge energy is relatively small. The main energy deposition process only last for ~ 4 μs. From the measured spectra, calibration curves for Pb, Mg and Sn in soil were derived and the limits of detection were 1.5 μg/g, 34 μg/g and 0.16 μg/g respectively.
doi_str_mv 10.1016/j.optcom.2011.08.074
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subjects Deposition
Electric discharges
Fast pulse discharge plasma
Laser ablation
Lead (metal)
LIBS
Magnesium
Soil (material)
Soil analysis
Spectroscopy
Tin
title Laser ablation fast pulse discharge plasma spectroscopy analysis of Pb, Mg and Sn in soil
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