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Structural characterization of self-assembled ZnO nanoparticles obtained by the sol–gel method from Zn(CH3COO)2·2H2O
Zinc oxide nanopowders were synthesized by the sol-gel method from an ethanol solution of zinc acetate dihydrate. Detailed structural and microstructural investigations were carried out using x-ray diffraction, Raman spectroscopy, thermogravimetric and differential thermal analyses, as well as high-...
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| Published in: | Nanotechnology 2011-09, Vol.22 (39), p.395603-395603 |
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| Main Authors: | , , , , , , , , , |
| Format: | Article |
| Language: | English |
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| container_end_page | 395603 |
| container_issue | 39 |
| container_start_page | 395603 |
| container_title | Nanotechnology |
| container_volume | 22 |
| creator | Luković Golić, D Branković, G Počuča Nešić, M Vojisavljević, K Rečnik, A Daneu, N Bernik, S Šćepanović, M Poleti, D Branković, Z |
| description | Zinc oxide nanopowders were synthesized by the sol-gel method from an ethanol solution of zinc acetate dihydrate. Detailed structural and microstructural investigations were carried out using x-ray diffraction, Raman spectroscopy, thermogravimetric and differential thermal analyses, as well as high-resolution transmission electron microscopy (TEM) and field-emission scanning electron microscopy. The intermediate compound of the reaction was layered zinc hydroxide acetate that further transforms into hexagonally shaped ZnO crystalline nanoplates (d(m) = 4 nm), which aggregate into larger spherical particles. According to the TEM analysis the ZnO nanoparticles were self-assembled into larger particles with the same orientation, i.e. aligned lattice planes of the particles. A further solvothermal treatment resulted in hexagonal, prismatic ZnO mesocrystals. |
| doi_str_mv | 10.1088/0957-4484/22/39/395603 |
| format | article |
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| title | Structural characterization of self-assembled ZnO nanoparticles obtained by the sol–gel method from Zn(CH3COO)2·2H2O |
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