Controlled solvothermal synthesis of novel organic functionalized polyoxovanadates

Four novel organic functionalized polyoxovanadates are solvothermally synthesized by altering the reaction temperature and using different organoarsonic acids. These POVs are fully characterized and the phase transitions between different POVs structures are confirmed by X-ray diffraction analyses....

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Bibliographic Details
Published in:Dalton transactions : an international journal of inorganic chemistry 2012-06, Vol.41 (23), p.691-6913
Main Authors: Chen, Baokuan, Wang, Bo, Lin, Zhengguo, Fan, Linyuan, Gao, Yuanzhe, Chi, Yingnan, Hu, Changwen
Format: Article
Language:English
Subjects:
Controlled atmospheres
Diffraction
Phase transformations
Synthesis
X-rays
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Summary:Four novel organic functionalized polyoxovanadates are solvothermally synthesized by altering the reaction temperature and using different organoarsonic acids. These POVs are fully characterized and the phase transitions between different POVs structures are confirmed by X-ray diffraction analyses. Such a transition is temperature-dependent and thus controlled synthesis of new POVs can be achieved. Four novel organic functionalized polyoxovanadates are solvothermally synthesized by altering the reaction temperature and by using different organoarsonic acids.
ISSN:1477-9226
1477-9234
DOI:10.1039/c2dt30660c