High-throughput synthesis and characterization of nanocrystalline porphyrinic zirconium metal-organic frameworks

We describe and employ a high-throughput screening method to accelerate the synthesis and identification of pure-phase, nanocrystalline metal-organic frameworks (MOFs). We demonstrate the efficacy of this method through its application to a series of porphyrinic zirconium MOFs, resulting in the isol...

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Bibliographic Details
Published in:Chemical communications (Cambridge, England) England), 2016-06, Vol.52 (5), p.7854-7857
Main Authors: Kelty, M. L, Morris, W, Gallagher, A. T, Anderson, J. S, Brown, K. A, Mirkin, C. A, Harris, T. D
Format: Article
Language:English
Subjects:
Effectiveness
Metal-organic frameworks
Nanocrystals
Nanostructure
Screening
Synthesis
Zirconium
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Summary:We describe and employ a high-throughput screening method to accelerate the synthesis and identification of pure-phase, nanocrystalline metal-organic frameworks (MOFs). We demonstrate the efficacy of this method through its application to a series of porphyrinic zirconium MOFs, resulting in the isolation of MOF-525, MOF-545, and PCN-223 on the nanoscale. We describe and employ a high-throughput screening method to accelerate the synthesis and identification of pure-phase, nanocrystalline metal-organic frameworks (MOFs).
ISSN:1359-7345
1364-548X
DOI:10.1039/c6cc03264h