First characterization of chemical environments using energy dispersive inelastic x-ray scattering induced by an x-ray tube

Energy Dispersive Inelastic X-ray Scattering (EDIXS) is a reliable technique for the discrimination and characterization of local chemical environments. By means of this methodology, the speciation of samples has been attained in a variety of samples and experimental conditions, such as total reflec...

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Published in:Review of scientific instruments 2021-01, Vol.92 (1), p.013102-013102
Main Authors: Pérez, Roberto Daniel, Leani, Juan José, Robledo, José Ignacio, Sánchez, Héctor Jorge
Format: Article
Language:English
Subjects:
Discrimination
Dispersion
Inelastic scattering
Iron compounds
Radiation sources
Scientific apparatus & instruments
Speciation
Synchrotron radiation
Synchrotrons
X ray tubes
X-ray scattering
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creator Pérez, Roberto Daniel
Leani, Juan José
Robledo, José Ignacio
Sánchez, Héctor Jorge
description Energy Dispersive Inelastic X-ray Scattering (EDIXS) is a reliable technique for the discrimination and characterization of local chemical environments. By means of this methodology, the speciation of samples has been attained in a variety of samples and experimental conditions, such as total reflection, grazing incidence, and confocal setups. Until now, due to the requirement of a monochromatic and intense exciting beam, this tool had been applied using exclusively synchrotron radiation sources. We present, for the first time, results of test measurements using EDIXS for chemical characterization implemented in a conventional x-ray tube based laboratory. The results show good discrimination between different iron compounds under study, suggesting the real possibility of rutinary chemical state characterizations of samples by means of EDIXS using a conventional x-ray tube.
doi_str_mv 10.1063/5.0026061
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source American Institute of Physics:Jisc Collections:Transitional Journals Agreement 2021-23 (Reading list); American Institute of Physics(アメリカ物理学協会)
subjects Discrimination
Dispersion
Inelastic scattering
Iron compounds
Radiation sources
Scientific apparatus & instruments
Speciation
Synchrotron radiation
Synchrotrons
X ray tubes
X-ray scattering
title First characterization of chemical environments using energy dispersive inelastic x-ray scattering induced by an x-ray tube
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