Synthesis, properties and antibacterial activity of Ca doped Zn 2 SnO 4 nanoparticles by microwave assisted method

A major problem in world health care is the development of antibiotic resistance in bacteria. In light of this, pure and calcium-doped zinc tin oxide (ZTO) nanoparticles, Zn SnO (S ), Zn Sn Ca O (S ), Zn Sn Ca O (S ), and Zn Sn Ca O (S ), were synthesized via simple and cost effective microwave assi...

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Published in:Applied physics. A, Materials science & processing Materials science & processing, 2023, Vol.129 (2), p.154
Main Authors: Pandimurugan, A R, Prasath, G Vijaya, Usha, K S, Vivekanandan, J, Karthikeyan, C, Sankaranarayanan, K, Ravi, G
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container_title Applied physics. A, Materials science & processing
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Prasath, G Vijaya
Usha, K S
Vivekanandan, J
Karthikeyan, C
Sankaranarayanan, K
Ravi, G
description A major problem in world health care is the development of antibiotic resistance in bacteria. In light of this, pure and calcium-doped zinc tin oxide (ZTO) nanoparticles, Zn SnO (S ), Zn Sn Ca O (S ), Zn Sn Ca O (S ), and Zn Sn Ca O (S ), were synthesized via simple and cost effective microwave assisted method. The doping effect on antibacterial activity was studied in detail. The XRD spectrum revealed that all the deposited samples exhibited a spinel cubic structure. A decrease in crystallite size, an increase in strain and dislocation density was observed with an increase in Ca concentration. FESEM images exhibited an irregular and non-homogeneous nature with crystalline morphology having a physical dimension of nm size. EDAX confirmed the purity of deposited samples. We used the agar well diffusion technique to study the antibacterial activity of Gram-positive and Gram-negative bacteria. The doping of the ZTO matrix with Ca ions increased its antibacterial performance by 99% against bacteria, and its effectiveness was enhanced with increasing Ca ion concentration inside the Zn SnO nanoparticles.
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In light of this, pure and calcium-doped zinc tin oxide (ZTO) nanoparticles, Zn SnO (S ), Zn Sn Ca O (S ), Zn Sn Ca O (S ), and Zn Sn Ca O (S ), were synthesized via simple and cost effective microwave assisted method. The doping effect on antibacterial activity was studied in detail. The XRD spectrum revealed that all the deposited samples exhibited a spinel cubic structure. A decrease in crystallite size, an increase in strain and dislocation density was observed with an increase in Ca concentration. FESEM images exhibited an irregular and non-homogeneous nature with crystalline morphology having a physical dimension of nm size. EDAX confirmed the purity of deposited samples. We used the agar well diffusion technique to study the antibacterial activity of Gram-positive and Gram-negative bacteria. 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