Indium K α radiation from a MetalJet X-ray source: the long way to a successful charge-density investigation

The MetalJet X-ray source provides indium α radiation with a wavelength even shorter than Ag radiation. This paper reports on problematic spectral impurities and presents possible countermeasures so that collection of data with excellent quality up to a high resolution is possible. It is demonstrate...

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Bibliographic Details
Published in:Journal of applied crystallography 2023-10, Vol.56 (Pt 5), p.1315-1321
Main Authors: Graw, Nico, Ruth, Paul Niklas, Ernemann, Tobias, Herbst-Irmer, Regine, Stalke, Dietmar
Format: Article
Language:English
Subjects:
Data collection
Impurities
Indium
Multipoles
Research Papers
Sulfur
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Summary:The MetalJet X-ray source provides indium α radiation with a wavelength even shorter than Ag radiation. This paper reports on problematic spectral impurities and presents possible countermeasures so that collection of data with excellent quality up to a high resolution is possible. It is demonstrated that these data can be used in the refinement of a multipole model, the results of which are used for a topological analysis to assess the bonding situation in a sulfur ylide compound.
ISSN:0021-8898
1600-5767
1600-5767
DOI:10.1107/S1600576723007203