Sealed rotors for in situ high temperature high pressure MAS NMR

Here we present the design of reusable and perfectly sealed all-zirconia MAS rotors. The rotors are used to study AlPO4-5 molecular sieve crystallization under hydrothermal conditions, high temperature high pressure cyclohexanol dehydration reaction, and low temperature metabolomics of intact biolog...

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Bibliographic Details
Published in:Chemical communications (Cambridge, England) England), 2015-01, Vol.51 (70), p.13458-13461
Main Authors: Hu, Jian Zhi, Hu, Mary Y, Zhao, Zhenchao, Xu, Suochang, Vjunov, Aleksei, Shi, Hui, Camaioni, Donald M, Peden, Charles H F, Lercher, Johannes A
Format: Article
Language:English
Subjects:
Biological
Chemistry Techniques, Analytical - instrumentation
Crystallization
Dehydration
ENGINEERING
Environmental Molecular Sciences Laboratory
Hot Temperature
Magnetic Resonance Spectroscopy - instrumentation
MATERIALS SCIENCE
Molecular sieves
NMR spectroscopy
Pressure
Reusable
Rotors
Zirconium - chemistry
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Summary:Here we present the design of reusable and perfectly sealed all-zirconia MAS rotors. The rotors are used to study AlPO4-5 molecular sieve crystallization under hydrothermal conditions, high temperature high pressure cyclohexanol dehydration reaction, and low temperature metabolomics of intact biological tissue.
ISSN:1359-7345
1364-548X
DOI:10.1039/c5cc03910j