Processing of Bulk Nanocrystalline Metals at the US Army Research Laboratory

• Published in: Journal of visualized experiments 2018-03 (133)
• Main Authors: Hammond, Vincent H, Hornbuckle, Billy C, Giri, Anit K, Roberts, Anthony J, Luckenbaugh, Thomas L, Marsico, Joseph M, Grendahl, Scott M, Darling, Kristopher A
• Format: Article
• Language: English
• Subjects: Academies and Institutes - standards; Crystallization - methods; Engineering; Hospitals, Military - standards; Laboratories - standards; Materials Testing - methods; United States
• ISSN: 1940-087X; 1940-087X
• DOI: 10.3791/56950

Given their potential for significant property improvements relative to their large grained counterparts, much work has been devoted to the continued development of nanocrystalline metals. Despite these efforts, the transition of these materials from the lab bench to actual applications has been blocked by the inability to produce large scale parts that retain the desired nanocrystalline microstructures. Following the development of a method proven to stabilize the nanosized grain structure to temperatures approaching that of the melting point for the given metal, the US Army Research Laboratory (ARL) has progressed to the next stage in the development of these materials - namely the production of large scale parts suitable for testing and evaluation in a range of relevant test environments. This report provides a broad overview of the ongoing efforts in the processing, characterization, and consolidation of these materials at ARL. In particular, focus is placed on the methodology used for producing the nanocrystalline metal powders, in both small and large-scale amounts, that are at the center of ongoing research efforts.