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Microstructure Evolution, Constitutive Modelling, and Superplastic Forming of Experimental 6XXX-Type Alloys Processed with Different Thermomechanical Treatments
This study focused on the microstructural analysis, superplasticity, modeling of superplastic deformation behavior, and superplastic forming tests of the Al-Mg-Si-Cu-based alloy modified with Fe, Ni, Sc, and Zr. The effect of the thermomechanical treatment with various proportions of hot/cold rollin...
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Published in: | Materials 2023-01, Vol.16 (1), p.445 |
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description | This study focused on the microstructural analysis, superplasticity, modeling of superplastic deformation behavior, and superplastic forming tests of the Al-Mg-Si-Cu-based alloy modified with Fe, Ni, Sc, and Zr. The effect of the thermomechanical treatment with various proportions of hot/cold rolling degrees on the secondary particle distribution and deformation behavior was studied. The increase in hot rolling degree increased the homogeneity of the particle distribution in the aluminum-based solid solution that improved superplastic properties, providing an elongation of ~470-500% at increased strain rates of (0.5-1) × 10
s
. A constitutive model based on Arrhenius and Beckofen equations was used to describe and predict the superplastic flow behavior of the alloy studied. Model complex-shaped parts were processed by superplastic forming at two strain rates. The proposed strain rate of 1 × 10
s
provided a low thickness variation and a high quality of the experimental parts. The residual cavitation after superplastic forming was also large at the low strain rate of 2 × 10
s
and significantly smaller at 1 × 10
s
. Coarse Al
FeNi particles did not stimulate the cavitation process and were effective to provide the superplasticity of alloys studied at high strain rates, whereas cavities were predominately observed near coarse Mg
Si particles, which act as nucleation places for cavities during superplastic deformation and forming. |
doi_str_mv | 10.3390/ma16010445 |
format | article |
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s
. A constitutive model based on Arrhenius and Beckofen equations was used to describe and predict the superplastic flow behavior of the alloy studied. Model complex-shaped parts were processed by superplastic forming at two strain rates. The proposed strain rate of 1 × 10
s
provided a low thickness variation and a high quality of the experimental parts. The residual cavitation after superplastic forming was also large at the low strain rate of 2 × 10
s
and significantly smaller at 1 × 10
s
. Coarse Al
FeNi particles did not stimulate the cavitation process and were effective to provide the superplasticity of alloys studied at high strain rates, whereas cavities were predominately observed near coarse Mg
Si particles, which act as nucleation places for cavities during superplastic deformation and forming.</description><identifier>ISSN: 1996-1944</identifier><identifier>EISSN: 1996-1944</identifier><identifier>DOI: 10.3390/ma16010445</identifier><identifier>PMID: 36614782</identifier><language>eng</language><publisher>Switzerland: MDPI AG</publisher><subject>Alloys ; Aluminum ; Aluminum base alloys ; Annealing ; Cavitation ; Cold ; Cold rolling ; Constitutive models ; Cooling ; Copper ; Copper base alloys ; Deformation ; Elongation ; Grain growth ; Grain size ; High strain rate ; Homogeneity ; Hot rolling ; Iron ; Magnesium compounds ; Mathematical models ; Metal silicides ; Microstructural analysis ; Microstructure ; Nucleation ; Scanning electron microscopy ; Silicon ; Solid solutions ; Specialty metals industry ; Superplastic deformation ; Superplastic forming ; Superplasticity ; Thermomechanical treatment ; Zirconium</subject><ispartof>Materials, 2023-01, Vol.16 (1), p.445</ispartof><rights>COPYRIGHT 2023 MDPI AG</rights><rights>2023 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><rights>2023 by the authors. 2023</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c375t-b983d644417571b0ffd693b6ee72390f455e13a5a9017ffa93038687e14e76133</citedby><cites>FETCH-LOGICAL-c375t-b983d644417571b0ffd693b6ee72390f455e13a5a9017ffa93038687e14e76133</cites><orcidid>0000-0001-7646-2883 ; 0000-0002-0247-7975 ; 0000-0001-5152-0477</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.proquest.com/docview/2761190399/fulltextPDF?pq-origsite=primo$$EPDF$$P50$$Gproquest$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.proquest.com/docview/2761190399?pq-origsite=primo$$EHTML$$P50$$Gproquest$$Hfree_for_read</linktohtml><link.rule.ids>230,314,723,776,780,881,25732,27903,27904,36991,36992,44569,53769,53771,74872</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/36614782$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Mochugovskiy, Andrey G</creatorcontrib><creatorcontrib>Mosleh, Ahmed O</creatorcontrib><creatorcontrib>Kotov, Anton D</creatorcontrib><creatorcontrib>Khokhlov, Andrey V</creatorcontrib><creatorcontrib>Kaplanskaya, Ludmila Yu</creatorcontrib><creatorcontrib>Mikhaylovskaya, Anastasia V</creatorcontrib><title>Microstructure Evolution, Constitutive Modelling, and Superplastic Forming of Experimental 6XXX-Type Alloys Processed with Different Thermomechanical Treatments</title><title>Materials</title><addtitle>Materials (Basel)</addtitle><description>This study focused on the microstructural analysis, superplasticity, modeling of superplastic deformation behavior, and superplastic forming tests of the Al-Mg-Si-Cu-based alloy modified with Fe, Ni, Sc, and Zr. The effect of the thermomechanical treatment with various proportions of hot/cold rolling degrees on the secondary particle distribution and deformation behavior was studied. The increase in hot rolling degree increased the homogeneity of the particle distribution in the aluminum-based solid solution that improved superplastic properties, providing an elongation of ~470-500% at increased strain rates of (0.5-1) × 10
s
. A constitutive model based on Arrhenius and Beckofen equations was used to describe and predict the superplastic flow behavior of the alloy studied. Model complex-shaped parts were processed by superplastic forming at two strain rates. The proposed strain rate of 1 × 10
s
provided a low thickness variation and a high quality of the experimental parts. The residual cavitation after superplastic forming was also large at the low strain rate of 2 × 10
s
and significantly smaller at 1 × 10
s
. Coarse Al
FeNi particles did not stimulate the cavitation process and were effective to provide the superplasticity of alloys studied at high strain rates, whereas cavities were predominately observed near coarse Mg
Si particles, which act as nucleation places for cavities during superplastic deformation and forming.</description><subject>Alloys</subject><subject>Aluminum</subject><subject>Aluminum base alloys</subject><subject>Annealing</subject><subject>Cavitation</subject><subject>Cold</subject><subject>Cold rolling</subject><subject>Constitutive models</subject><subject>Cooling</subject><subject>Copper</subject><subject>Copper base alloys</subject><subject>Deformation</subject><subject>Elongation</subject><subject>Grain growth</subject><subject>Grain size</subject><subject>High strain rate</subject><subject>Homogeneity</subject><subject>Hot rolling</subject><subject>Iron</subject><subject>Magnesium compounds</subject><subject>Mathematical models</subject><subject>Metal silicides</subject><subject>Microstructural analysis</subject><subject>Microstructure</subject><subject>Nucleation</subject><subject>Scanning electron microscopy</subject><subject>Silicon</subject><subject>Solid solutions</subject><subject>Specialty metals industry</subject><subject>Superplastic deformation</subject><subject>Superplastic forming</subject><subject>Superplasticity</subject><subject>Thermomechanical treatment</subject><subject>Zirconium</subject><issn>1996-1944</issn><issn>1996-1944</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><sourceid>PIMPY</sourceid><recordid>eNpdklFvFCEQxzdGY5vaFz-AIfHFmG6FhWWXF5PLeVWTNpp4Jve24djhjoaFE9jT-zZ-VFmv1io8AMNv_sMMUxTPCb6kVOA3gyQcE8xY_ag4JULwkgjGHj_YnxTnMd7iPCglbSWeFieUc8Katjotft4YFXxMYVRpDIAWe2_HZLy7QHPvYjIpn_aAbnwP1hq3uUDS9ejLuIOwszIDCl35MOQb5DVa_Mh2M4BL0iK-Wq3K5WEHaGatP0T0OXgFMUKPvpu0Re-M1hAyi5ZbCIMfQG2lMyq7LgPINMnEZ8UTLW2E87v1rPh6tVjOP5TXn95_nM-uS0WbOpVr0dKeM8ZIUzdkjbXuuaBrDtBUuUya1TUQKmspMGm0loJi2vK2AcKg4YTSs-LtUXc3rgfoVY4dpO12ORsZDp2Xpvv3xpltt_H7TrRVruok8OpOIPhvI8TUDSaqXDTpwI-xq3IY0WLC24y-_A-99WNwOb3fFBGYCpGpyyO1kRY647TPcVWePQxGeQfaZPusYZTUgreTw-ujw_SjMYC-fz3B3dQs3d9myfCLh_neo39ag_4CFBK8mQ</recordid><startdate>20230103</startdate><enddate>20230103</enddate><creator>Mochugovskiy, Andrey G</creator><creator>Mosleh, Ahmed O</creator><creator>Kotov, Anton D</creator><creator>Khokhlov, Andrey V</creator><creator>Kaplanskaya, Ludmila Yu</creator><creator>Mikhaylovskaya, Anastasia V</creator><general>MDPI AG</general><general>MDPI</general><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>7X8</scope><scope>5PM</scope><orcidid>https://orcid.org/0000-0001-7646-2883</orcidid><orcidid>https://orcid.org/0000-0002-0247-7975</orcidid><orcidid>https://orcid.org/0000-0001-5152-0477</orcidid></search><sort><creationdate>20230103</creationdate><title>Microstructure Evolution, Constitutive Modelling, and Superplastic Forming of Experimental 6XXX-Type Alloys Processed with Different Thermomechanical Treatments</title><author>Mochugovskiy, Andrey G ; Mosleh, Ahmed O ; Kotov, Anton D ; Khokhlov, Andrey V ; Kaplanskaya, Ludmila Yu ; Mikhaylovskaya, Anastasia V</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c375t-b983d644417571b0ffd693b6ee72390f455e13a5a9017ffa93038687e14e76133</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Alloys</topic><topic>Aluminum</topic><topic>Aluminum base alloys</topic><topic>Annealing</topic><topic>Cavitation</topic><topic>Cold</topic><topic>Cold rolling</topic><topic>Constitutive models</topic><topic>Cooling</topic><topic>Copper</topic><topic>Copper base alloys</topic><topic>Deformation</topic><topic>Elongation</topic><topic>Grain growth</topic><topic>Grain size</topic><topic>High strain rate</topic><topic>Homogeneity</topic><topic>Hot rolling</topic><topic>Iron</topic><topic>Magnesium compounds</topic><topic>Mathematical models</topic><topic>Metal silicides</topic><topic>Microstructural analysis</topic><topic>Microstructure</topic><topic>Nucleation</topic><topic>Scanning electron microscopy</topic><topic>Silicon</topic><topic>Solid solutions</topic><topic>Specialty metals industry</topic><topic>Superplastic deformation</topic><topic>Superplastic forming</topic><topic>Superplasticity</topic><topic>Thermomechanical treatment</topic><topic>Zirconium</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Mochugovskiy, Andrey G</creatorcontrib><creatorcontrib>Mosleh, Ahmed O</creatorcontrib><creatorcontrib>Kotov, Anton D</creatorcontrib><creatorcontrib>Khokhlov, Andrey V</creatorcontrib><creatorcontrib>Kaplanskaya, Ludmila Yu</creatorcontrib><creatorcontrib>Mikhaylovskaya, Anastasia V</creatorcontrib><collection>PubMed</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni)</collection><collection>ProQuest Central</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Materials Science Collection</collection><collection>Publicly Available Content Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>MEDLINE - Academic</collection><collection>PubMed Central (Full Participant titles)</collection><jtitle>Materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Mochugovskiy, Andrey G</au><au>Mosleh, Ahmed O</au><au>Kotov, Anton D</au><au>Khokhlov, Andrey V</au><au>Kaplanskaya, Ludmila Yu</au><au>Mikhaylovskaya, Anastasia V</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Microstructure Evolution, Constitutive Modelling, and Superplastic Forming of Experimental 6XXX-Type Alloys Processed with Different Thermomechanical Treatments</atitle><jtitle>Materials</jtitle><addtitle>Materials (Basel)</addtitle><date>2023-01-03</date><risdate>2023</risdate><volume>16</volume><issue>1</issue><spage>445</spage><pages>445-</pages><issn>1996-1944</issn><eissn>1996-1944</eissn><abstract>This study focused on the microstructural analysis, superplasticity, modeling of superplastic deformation behavior, and superplastic forming tests of the Al-Mg-Si-Cu-based alloy modified with Fe, Ni, Sc, and Zr. The effect of the thermomechanical treatment with various proportions of hot/cold rolling degrees on the secondary particle distribution and deformation behavior was studied. The increase in hot rolling degree increased the homogeneity of the particle distribution in the aluminum-based solid solution that improved superplastic properties, providing an elongation of ~470-500% at increased strain rates of (0.5-1) × 10
s
. A constitutive model based on Arrhenius and Beckofen equations was used to describe and predict the superplastic flow behavior of the alloy studied. Model complex-shaped parts were processed by superplastic forming at two strain rates. The proposed strain rate of 1 × 10
s
provided a low thickness variation and a high quality of the experimental parts. The residual cavitation after superplastic forming was also large at the low strain rate of 2 × 10
s
and significantly smaller at 1 × 10
s
. Coarse Al
FeNi particles did not stimulate the cavitation process and were effective to provide the superplasticity of alloys studied at high strain rates, whereas cavities were predominately observed near coarse Mg
Si particles, which act as nucleation places for cavities during superplastic deformation and forming.</abstract><cop>Switzerland</cop><pub>MDPI AG</pub><pmid>36614782</pmid><doi>10.3390/ma16010445</doi><orcidid>https://orcid.org/0000-0001-7646-2883</orcidid><orcidid>https://orcid.org/0000-0002-0247-7975</orcidid><orcidid>https://orcid.org/0000-0001-5152-0477</orcidid><oa>free_for_read</oa></addata></record> |
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language | eng |
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source | Publicly Available Content Database; PubMed Central; Free Full-Text Journals in Chemistry |
subjects | Alloys Aluminum Aluminum base alloys Annealing Cavitation Cold Cold rolling Constitutive models Cooling Copper Copper base alloys Deformation Elongation Grain growth Grain size High strain rate Homogeneity Hot rolling Iron Magnesium compounds Mathematical models Metal silicides Microstructural analysis Microstructure Nucleation Scanning electron microscopy Silicon Solid solutions Specialty metals industry Superplastic deformation Superplastic forming Superplasticity Thermomechanical treatment Zirconium |
title | Microstructure Evolution, Constitutive Modelling, and Superplastic Forming of Experimental 6XXX-Type Alloys Processed with Different Thermomechanical Treatments |
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