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Effects of Gas Nitriding on Fatigue and Crack Initiation of Ti6Al4V produced by Selective Laser Melting
Selective laser melting (SLM) is an additive manufacturing technique which permits fabrication of three dimensional parts by selectively melting consecutive layers of metallic powder. This allows the production of parts with high geometrical complexity. Titanium alloy Ti-6Al-4V (Ti64) is widely used...
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Published in: | Materials research (São Carlos, São Paulo, Brazil) São Paulo, Brazil), 2019, Vol.22 (suppl 2), p.1 |
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description | Selective laser melting (SLM) is an additive manufacturing technique which permits fabrication of three dimensional parts by selectively melting consecutive layers of metallic powder. This allows the production of parts with high geometrical complexity. Titanium alloy Ti-6Al-4V (Ti64) is widely used in industry due to its high strength-to-mass ratio, corrosion resistance and biocompatibility. SLM increases the application range of Ti64 because of its flexibility for prototyping any part and its low material waste. Nitriding is a diffusion-based thermo-chemical treatment for interstitial hardening of the surface of Ti64 alloy products. This study characterized the fatigue behaviour of SLM-produced Ti64 nitrided and annealed bars in as-built and machined surface conditions. The surface of the SLM-produced Ti64 parts after gas nitriding showed high values of micro-hardness up to 550 HV just below the surface. Fatigue testing was performed to assess the materials fatigue strength and fractographic imaging was used to examine fracture surface and nitride layer characteristics. Nitriding was found to reduce the fatigue strength of the samples to a similar level irrespective of being in the as-built or machined condition. The effect of nitriding on crack initiation and growth at various stress levels under fatigue loading was investigated. |
doi_str_mv | 10.1590/1980-5373-mr-2018-0766 |
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This allows the production of parts with high geometrical complexity. Titanium alloy Ti-6Al-4V (Ti64) is widely used in industry due to its high strength-to-mass ratio, corrosion resistance and biocompatibility. SLM increases the application range of Ti64 because of its flexibility for prototyping any part and its low material waste. Nitriding is a diffusion-based thermo-chemical treatment for interstitial hardening of the surface of Ti64 alloy products. This study characterized the fatigue behaviour of SLM-produced Ti64 nitrided and annealed bars in as-built and machined surface conditions. The surface of the SLM-produced Ti64 parts after gas nitriding showed high values of micro-hardness up to 550 HV just below the surface. Fatigue testing was performed to assess the materials fatigue strength and fractographic imaging was used to examine fracture surface and nitride layer characteristics. Nitriding was found to reduce the fatigue strength of the samples to a similar level irrespective of being in the as-built or machined condition. The effect of nitriding on crack initiation and growth at various stress levels under fatigue loading was investigated.</description><identifier>ISSN: 1516-1439</identifier><identifier>ISSN: 1980-5373</identifier><identifier>EISSN: 1980-5373</identifier><identifier>DOI: 10.1590/1980-5373-mr-2018-0766</identifier><language>eng</language><publisher>Sao Carlos: Universidade Federal do Sao Carlos, Departamento de Engenharia de Materiais</publisher><subject>Biocompatibility ; Chemical treatment ; Corrosion resistance ; Crack initiation ; Crack propagation ; ENGINEERING, CHEMICAL ; Fatigue ; Fatigue failure ; Fatigue strength ; Fatigue tests ; Fracture mechanics ; Fracture surfaces ; Gas nitriding ; Laser beam melting ; MATERIALS SCIENCE, MULTIDISCIPLINARY ; Metal powders ; METALLURGY & METALLURGICAL ENGINEERING ; Microhardness ; Nitriding ; Organic chemistry ; Prototyping ; Rapid prototyping ; Selective laser melting ; Titanium ; Titanium alloys ; Titanium base alloys</subject><ispartof>Materials research (São Carlos, São Paulo, Brazil), 2019, Vol.22 (suppl 2), p.1</ispartof><rights>Copyright Universidade Federal do Sao Carlos, Departamento de Engenharia de Materiais 2019</rights><rights>This work is licensed under a Creative Commons Attribution 4.0 International License.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c436t-4abb0842d458edbc1e892e69ff329fd7ce8e27571cbae4ab3c6c4d6b384ec85d3</citedby><cites>FETCH-LOGICAL-c436t-4abb0842d458edbc1e892e69ff329fd7ce8e27571cbae4ab3c6c4d6b384ec85d3</cites><orcidid>0000-0002-1467-4116</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>230,314,777,781,882,4010,24131,27904,27905,27906</link.rule.ids></links><search><creatorcontrib>Mukhtar, Aamir</creatorcontrib><creatorcontrib>Fry, Mike</creatorcontrib><creatorcontrib>Jackson, Ben</creatorcontrib><creatorcontrib>Bolzoni, Leandro</creatorcontrib><title>Effects of Gas Nitriding on Fatigue and Crack Initiation of Ti6Al4V produced by Selective Laser Melting</title><title>Materials research (São Carlos, São Paulo, Brazil)</title><addtitle>Mat. Res</addtitle><description>Selective laser melting (SLM) is an additive manufacturing technique which permits fabrication of three dimensional parts by selectively melting consecutive layers of metallic powder. This allows the production of parts with high geometrical complexity. Titanium alloy Ti-6Al-4V (Ti64) is widely used in industry due to its high strength-to-mass ratio, corrosion resistance and biocompatibility. SLM increases the application range of Ti64 because of its flexibility for prototyping any part and its low material waste. Nitriding is a diffusion-based thermo-chemical treatment for interstitial hardening of the surface of Ti64 alloy products. This study characterized the fatigue behaviour of SLM-produced Ti64 nitrided and annealed bars in as-built and machined surface conditions. The surface of the SLM-produced Ti64 parts after gas nitriding showed high values of micro-hardness up to 550 HV just below the surface. Fatigue testing was performed to assess the materials fatigue strength and fractographic imaging was used to examine fracture surface and nitride layer characteristics. Nitriding was found to reduce the fatigue strength of the samples to a similar level irrespective of being in the as-built or machined condition. The effect of nitriding on crack initiation and growth at various stress levels under fatigue loading was investigated.</description><subject>Biocompatibility</subject><subject>Chemical treatment</subject><subject>Corrosion resistance</subject><subject>Crack initiation</subject><subject>Crack propagation</subject><subject>ENGINEERING, CHEMICAL</subject><subject>Fatigue</subject><subject>Fatigue failure</subject><subject>Fatigue strength</subject><subject>Fatigue tests</subject><subject>Fracture mechanics</subject><subject>Fracture surfaces</subject><subject>Gas nitriding</subject><subject>Laser beam melting</subject><subject>MATERIALS SCIENCE, MULTIDISCIPLINARY</subject><subject>Metal powders</subject><subject>METALLURGY & METALLURGICAL ENGINEERING</subject><subject>Microhardness</subject><subject>Nitriding</subject><subject>Organic chemistry</subject><subject>Prototyping</subject><subject>Rapid prototyping</subject><subject>Selective laser melting</subject><subject>Titanium</subject><subject>Titanium alloys</subject><subject>Titanium base alloys</subject><issn>1516-1439</issn><issn>1980-5373</issn><issn>1980-5373</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><sourceid>DOA</sourceid><recordid>eNpFkUlrHDEQhUWIIc7EfyEIcm5HW2s5msHLwMQ-eLkKtVQaNOlpOVJPwP8-6kxwTlVU1XsU30PoKyWXtDfkOzWadD1XvDuUjhGqO6Kk_IDO3xcfW99T2VHBzSf0udY9IUxxyc_R7jpG8HPFOeJbV_F9mksKadrhPOEbN6fdEbCbAl4X53_izZTm1KZt2QRPSV6N4gW_lhyOHgIe3vAjjM0v_Qa8dRUK_gHj3Oy-oLPoxgoX_-oKPd9cP63vuu3D7WZ9te284HLuhBsGogULotcQBk9BGwbSxMiZiUF50MBUr6gfHLRj7qUXQQ5cC_C6D3yFNiffkN3evpZ0cOXNZpfs30EuO-vKnPwIVhrjNSjwIILgig2GRGUoo4F5Jf3QvC5PXtUnGLPd52OZ2vP2caFpF5oNtyGE6MaTkib4dhI0IL-OUOf_EsakMLTXDfsKydOVL7nWAvH9TUrskqhdgrNLcPZQ7JKoXRLlfwBe7pG8</recordid><startdate>2019</startdate><enddate>2019</enddate><creator>Mukhtar, Aamir</creator><creator>Fry, Mike</creator><creator>Jackson, Ben</creator><creator>Bolzoni, Leandro</creator><general>Universidade Federal do Sao Carlos, Departamento de Engenharia de Materiais</general><general>ABM, ABC, ABPol</general><general>Associação Brasileira de Metalurgia e Materiais (ABM); Associação Brasileira de Cerâmica (ABC); Associação Brasileira de Polímeros (ABPol)</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>GPN</scope><scope>DOA</scope><orcidid>https://orcid.org/0000-0002-1467-4116</orcidid></search><sort><creationdate>2019</creationdate><title>Effects of Gas Nitriding on Fatigue and Crack Initiation of Ti6Al4V produced by Selective Laser Melting</title><author>Mukhtar, Aamir ; Fry, Mike ; Jackson, Ben ; Bolzoni, Leandro</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c436t-4abb0842d458edbc1e892e69ff329fd7ce8e27571cbae4ab3c6c4d6b384ec85d3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2019</creationdate><topic>Biocompatibility</topic><topic>Chemical treatment</topic><topic>Corrosion resistance</topic><topic>Crack initiation</topic><topic>Crack propagation</topic><topic>ENGINEERING, CHEMICAL</topic><topic>Fatigue</topic><topic>Fatigue failure</topic><topic>Fatigue strength</topic><topic>Fatigue tests</topic><topic>Fracture mechanics</topic><topic>Fracture surfaces</topic><topic>Gas nitriding</topic><topic>Laser beam melting</topic><topic>MATERIALS SCIENCE, MULTIDISCIPLINARY</topic><topic>Metal powders</topic><topic>METALLURGY & METALLURGICAL ENGINEERING</topic><topic>Microhardness</topic><topic>Nitriding</topic><topic>Organic chemistry</topic><topic>Prototyping</topic><topic>Rapid prototyping</topic><topic>Selective laser melting</topic><topic>Titanium</topic><topic>Titanium alloys</topic><topic>Titanium base alloys</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Mukhtar, Aamir</creatorcontrib><creatorcontrib>Fry, Mike</creatorcontrib><creatorcontrib>Jackson, Ben</creatorcontrib><creatorcontrib>Bolzoni, Leandro</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>SciELO</collection><collection>DOAJ Directory of Open Access Journals</collection><jtitle>Materials research (São Carlos, São Paulo, Brazil)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Mukhtar, Aamir</au><au>Fry, Mike</au><au>Jackson, Ben</au><au>Bolzoni, Leandro</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Effects of Gas Nitriding on Fatigue and Crack Initiation of Ti6Al4V produced by Selective Laser Melting</atitle><jtitle>Materials research (São Carlos, São Paulo, Brazil)</jtitle><addtitle>Mat. 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The surface of the SLM-produced Ti64 parts after gas nitriding showed high values of micro-hardness up to 550 HV just below the surface. Fatigue testing was performed to assess the materials fatigue strength and fractographic imaging was used to examine fracture surface and nitride layer characteristics. Nitriding was found to reduce the fatigue strength of the samples to a similar level irrespective of being in the as-built or machined condition. The effect of nitriding on crack initiation and growth at various stress levels under fatigue loading was investigated.</abstract><cop>Sao Carlos</cop><pub>Universidade Federal do Sao Carlos, Departamento de Engenharia de Materiais</pub><doi>10.1590/1980-5373-mr-2018-0766</doi><orcidid>https://orcid.org/0000-0002-1467-4116</orcidid><oa>free_for_read</oa></addata></record> |
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subjects | Biocompatibility Chemical treatment Corrosion resistance Crack initiation Crack propagation ENGINEERING, CHEMICAL Fatigue Fatigue failure Fatigue strength Fatigue tests Fracture mechanics Fracture surfaces Gas nitriding Laser beam melting MATERIALS SCIENCE, MULTIDISCIPLINARY Metal powders METALLURGY & METALLURGICAL ENGINEERING Microhardness Nitriding Organic chemistry Prototyping Rapid prototyping Selective laser melting Titanium Titanium alloys Titanium base alloys |
title | Effects of Gas Nitriding on Fatigue and Crack Initiation of Ti6Al4V produced by Selective Laser Melting |
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