NMR in a diamond anvil cell

Techniques are presented for NMR measurements at high pressure in a diamond anvil cell. Two schemes of coupling radio frequency magnetic fields to the spins inside a metal gasket are described. As a demonstration of the techniques, the relaxation times T 1 and T 2 of methanol:ethanol solution have b...

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Bibliographic Details
Published in:Review of scientific instruments 1987-03, Vol.58 (3), p.415-417
Main Authors: Lee, Sam‐Hyeon, Luszczynski, K., Norberg, R. E., Conradi, Mark S.
Format: Article
Language:English
Subjects:
Exact sciences and technology
Infrared, submillimeter wave, microwave and radiowave instruments, equipment and techniques
Instruments, apparatus, components and techniques common to several branches of physics and astronomy
Physics
Submillimeter wave, microwave and radiowave spectrometers
magnetic resonance spectrometers, auxiliary equipments and techniques
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Summary:Techniques are presented for NMR measurements at high pressure in a diamond anvil cell. Two schemes of coupling radio frequency magnetic fields to the spins inside a metal gasket are described. As a demonstration of the techniques, the relaxation times T 1 and T 2 of methanol:ethanol solution have been measured to 52 kbar at room temperature.
ISSN:0034-6748
1089-7623
DOI:10.1063/1.1139246