Synthesis and characterization of 1-(3-aminophenyl)-3-(naphthalen-1-yl)thiourea and preliminary study towards binding with metal ions

New mono-thiourea derivative, 1-(3-aminophenyl)-3-(naphthalen-1-yl)thiourea (3) has been synthesized from the reaction of 1-naphthyl isothiocyanate (1) and 1,3-phenylenediamine (2) using conventional method. The percentage yield of compound 3 was 82%. The compound 3 was characterized using FT-Infrar...

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Bibliographic Details
Main Authors: Ngah, Fatimatul Akma Awang, Heng, Lee Yook, Hassan, Nurul Izzaty, Hasbullah, Siti Aishah
Format: Conference Proceeding
Language:English
Subjects:
Binding
Chemical sensors
Chemical synthesis
Ions
Mass spectrometry
Metal ions
NMR
Nuclear magnetic resonance
Organic chemistry
Phenylenediamine
Thiourea derivatives
Thioureas
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Summary:New mono-thiourea derivative, 1-(3-aminophenyl)-3-(naphthalen-1-yl)thiourea (3) has been synthesized from the reaction of 1-naphthyl isothiocyanate (1) and 1,3-phenylenediamine (2) using conventional method. The percentage yield of compound 3 was 82%. The compound 3 was characterized using FT-Infrared (FT-IR), 1H and 1C Nuclear Magnetic Resonance (NMR) spectroscopies and Mass Spectrometry. An application of chemical sensor on this compound was prepared and examined by UV-vis spectrometer to study the binding interaction between metal ions and compound 3.
ISSN:0094-243X
1551-7616
DOI:10.1063/1.4966752