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Epoxidation of waste cooking oil by using homogeneous catalyst
The aim of this research is to study on epoxidation of waste cooking oil by application of in situ peracid mechanism. The epoxidation process was carried out by implementing in situ generated performic acid by using sulfuric acid as homogenous catalyst in order to produce epoxidized waste cooking oi...
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creator | Azmi, Intan Suhada Raofuddin, Danial Nuruddin Azlan Sharif, Muhammad Muain Md Jalil, Mohd Jumain |
description | The aim of this research is to study on epoxidation of waste cooking oil by application of in situ peracid mechanism. The epoxidation process was carried out by implementing in situ generated performic acid by using sulfuric acid as homogenous catalyst in order to produce epoxidized waste cooking oil. The reaction that occurred between formic acid and hydrogen peroxide will then produce performic acid. Formic acid was classified as oxygen carrier whereas hydrogen peroxide acts as oxygen donor. The main target of this work is to synthesis a high yield of epoxidized waste cooking oil and to investigates the influence of temperatures in term of relative conversion to oxirane (RCO). FTIR spectroscopy was used to proof the presence of oxirane ring in the epoxidized waste cooking oil. The FTIR findings shows that the oxirane ring was found at wavenumber 750-880 cm-1. The outcomes from this research showed that the highest percentage of RCO was 85% at the temperature of 55°C. |
doi_str_mv | 10.1063/5.0115008 |
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The epoxidation process was carried out by implementing in situ generated performic acid by using sulfuric acid as homogenous catalyst in order to produce epoxidized waste cooking oil. The reaction that occurred between formic acid and hydrogen peroxide will then produce performic acid. Formic acid was classified as oxygen carrier whereas hydrogen peroxide acts as oxygen donor. The main target of this work is to synthesis a high yield of epoxidized waste cooking oil and to investigates the influence of temperatures in term of relative conversion to oxirane (RCO). FTIR spectroscopy was used to proof the presence of oxirane ring in the epoxidized waste cooking oil. The FTIR findings shows that the oxirane ring was found at wavenumber 750-880 cm-1. The outcomes from this research showed that the highest percentage of RCO was 85% at the temperature of 55°C.</description><identifier>ISSN: 0094-243X</identifier><identifier>EISSN: 1551-7616</identifier><identifier>DOI: 10.1063/5.0115008</identifier><identifier>CODEN: APCPCS</identifier><language>eng</language><publisher>Melville: American Institute of Physics</publisher><subject>Catalysts ; Cooking ; Epoxidation ; Ethylene oxide ; Formic acid ; Fourier transforms ; Hydrogen peroxide ; Infrared spectroscopy ; Oxygen ; Peracids ; Sulfuric acid ; Wavelengths</subject><ispartof>AIP conference proceedings, 2023, Vol.2703 (1)</ispartof><rights>Author(s)</rights><rights>2023 Author(s). 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The outcomes from this research showed that the highest percentage of RCO was 85% at the temperature of 55°C.</description><subject>Catalysts</subject><subject>Cooking</subject><subject>Epoxidation</subject><subject>Ethylene oxide</subject><subject>Formic acid</subject><subject>Fourier transforms</subject><subject>Hydrogen peroxide</subject><subject>Infrared spectroscopy</subject><subject>Oxygen</subject><subject>Peracids</subject><subject>Sulfuric acid</subject><subject>Wavelengths</subject><issn>0094-243X</issn><issn>1551-7616</issn><fulltext>true</fulltext><rsrctype>conference_proceeding</rsrctype><creationdate>2023</creationdate><recordtype>conference_proceeding</recordtype><recordid>eNp9kMtKAzEUhoMoWC8L3yDgTpiaM5ncNoKUeoGCGwV3IZNLndpOxklG7dvb2oI7V4cD3_8fzofQBZAxEE6v2ZgAMELkARoBY1AIDvwQjQhRVVFW9PUYnaS0IKRUQsgRupl28btxJjexxTHgL5OyxzbG96ad49gscb3GQ9oub3EV5771cUjYmmyW65TP0FEwy-TP9_MUvdxNnycPxezp_nFyOys64DIXHMApJoMN1FtnjRCKVZWqHdDASkF4kIY5T6llklpTK29r4cASZSuQnNJTdLnr7fr4MfiU9SIOfbs5qUtZVlBS4GRDXe2oZJv8-5Lu-mZl-rX-jL1meu9Gdy78BwPRW5l_AfoDQnNmEA</recordid><startdate>20230609</startdate><enddate>20230609</enddate><creator>Azmi, Intan Suhada</creator><creator>Raofuddin, Danial Nuruddin Azlan</creator><creator>Sharif, Muhammad Muain Md</creator><creator>Jalil, Mohd Jumain</creator><general>American Institute of Physics</general><scope>8FD</scope><scope>H8D</scope><scope>L7M</scope></search><sort><creationdate>20230609</creationdate><title>Epoxidation of waste cooking oil by using homogeneous catalyst</title><author>Azmi, Intan Suhada ; Raofuddin, Danial Nuruddin Azlan ; Sharif, Muhammad Muain Md ; Jalil, Mohd Jumain</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-p168t-611d958fcf3ecdca7795449bd13f52706f8a5de33c583cab9ecb7d1c09c418633</frbrgroupid><rsrctype>conference_proceedings</rsrctype><prefilter>conference_proceedings</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Catalysts</topic><topic>Cooking</topic><topic>Epoxidation</topic><topic>Ethylene oxide</topic><topic>Formic acid</topic><topic>Fourier transforms</topic><topic>Hydrogen peroxide</topic><topic>Infrared spectroscopy</topic><topic>Oxygen</topic><topic>Peracids</topic><topic>Sulfuric acid</topic><topic>Wavelengths</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Azmi, Intan Suhada</creatorcontrib><creatorcontrib>Raofuddin, Danial Nuruddin Azlan</creatorcontrib><creatorcontrib>Sharif, Muhammad Muain Md</creatorcontrib><creatorcontrib>Jalil, Mohd Jumain</creatorcontrib><collection>Technology Research Database</collection><collection>Aerospace Database</collection><collection>Advanced Technologies Database with Aerospace</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Azmi, Intan Suhada</au><au>Raofuddin, Danial Nuruddin Azlan</au><au>Sharif, Muhammad Muain Md</au><au>Jalil, Mohd Jumain</au><au>Ghani, Azlinda Abdul</au><au>Khasri, Azduwin</au><au>Iberahim, Nur Izzati</au><au>Zainol, Noor Ainee</au><au>Rohaizad, Nor Munirah</au><au>Daud, Adibah Izzati</au><format>book</format><genre>proceeding</genre><ristype>CONF</ristype><atitle>Epoxidation of waste cooking oil by using homogeneous catalyst</atitle><btitle>AIP conference proceedings</btitle><date>2023-06-09</date><risdate>2023</risdate><volume>2703</volume><issue>1</issue><issn>0094-243X</issn><eissn>1551-7616</eissn><coden>APCPCS</coden><abstract>The aim of this research is to study on epoxidation of waste cooking oil by application of in situ peracid mechanism. The epoxidation process was carried out by implementing in situ generated performic acid by using sulfuric acid as homogenous catalyst in order to produce epoxidized waste cooking oil. The reaction that occurred between formic acid and hydrogen peroxide will then produce performic acid. Formic acid was classified as oxygen carrier whereas hydrogen peroxide acts as oxygen donor. The main target of this work is to synthesis a high yield of epoxidized waste cooking oil and to investigates the influence of temperatures in term of relative conversion to oxirane (RCO). FTIR spectroscopy was used to proof the presence of oxirane ring in the epoxidized waste cooking oil. The FTIR findings shows that the oxirane ring was found at wavenumber 750-880 cm-1. The outcomes from this research showed that the highest percentage of RCO was 85% at the temperature of 55°C.</abstract><cop>Melville</cop><pub>American Institute of Physics</pub><doi>10.1063/5.0115008</doi><tpages>6</tpages></addata></record> |
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identifier | ISSN: 0094-243X |
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language | eng |
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source | American Institute of Physics:Jisc Collections:Transitional Journals Agreement 2021-23 (Reading list) |
subjects | Catalysts Cooking Epoxidation Ethylene oxide Formic acid Fourier transforms Hydrogen peroxide Infrared spectroscopy Oxygen Peracids Sulfuric acid Wavelengths |
title | Epoxidation of waste cooking oil by using homogeneous catalyst |
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