Evaluation of solid-phase extraction sorbent with ketoimine groups for the preconcentration of benzene and phenolic compounds in water

The applicability of silica gel, modified with ketoimine groups, to solid phase extraction (SPE) was tested. Basic characteristics of the modified silica were determined using elemental analysis, $and^ {29}$ Si CP MAS NMR spectroscopy, as well as measurement of specific surface area. Some applicatio...

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Bibliographic Details
Published in:Turkish journal of chemistry 2010-01, Vol.34 (3), p.457-464
Main Authors: RYKOWSKA, IWONA, WASIAK, WIESLAW
Format: Article
Language:English
Online Access:Get full text
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Summary:The applicability of silica gel, modified with ketoimine groups, to solid phase extraction (SPE) was tested. Basic characteristics of the modified silica were determined using elemental analysis, $and^ {29}$ Si CP MAS NMR spectroscopy, as well as measurement of specific surface area. Some applications of the sorbent studied to preconcentration and further determination of organic compounds, such as benzene, phenol, and o-chlorophenol, by means of solid-phase extraction (SPE) and gas chromatography are presented. The determined recovery rates were about 95%-98%.
ISSN:1303-6130
1300-0527
1303-6130
DOI:10.3906/kim-0909-261