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Synthesis of a NiTi2-AlNi-Al2O3 nanocomposite by mechanical alloying and heat treatment of Al-TiO2-NiO

The aim of the present study was to investigate the phases formed during ball milling of Al-TiO 2 -NiO. For this purpose, a mixture of Al-TiO 2 -NiO with a molar ratio of 6:1:1 was used. Characterization of the milled powders by X-ray diffraction, differential thermal analysis, field-emission scanni...

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Published in:International journal of minerals, metallurgy and materials metallurgy and materials, 2019-03, Vol.26 (3), p.345-349
Main Authors: Beygi, Reza, Mehrizi, Majid Zarezadeh, Mostaan, Hossein, Rafiei, Mahdi, Abbasian, Ahmadreza
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description The aim of the present study was to investigate the phases formed during ball milling of Al-TiO 2 -NiO. For this purpose, a mixture of Al-TiO 2 -NiO with a molar ratio of 6:1:1 was used. Characterization of the milled powders by X-ray diffraction, differential thermal analysis, field-emission scanning electron microscopy, and transmission electron microscopy showed the formation of nanocrystalline NiTi 2 along with AlNi. A thermodynamical investigation confirmed that NiO was reduced by Al during ball milling, which consequently promoted TiO 2 reduction and the formation of NiTi 2 . Al is capable of reducing NiO either during ball milling or at temperatures above the melting point of Al; by contrast, TiO 2 can be reduced by Al only by milling.
doi_str_mv 10.1007/s12613-019-1743-7
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ispartof International journal of minerals, metallurgy and materials, 2019-03, Vol.26 (3), p.345-349
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language eng
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source Springer Nature
subjects Aluminum oxide
Ball milling
Ceramics
Characterization and Evaluation of Materials
Chemistry and Materials Science
Chromium steel
Composites
Corrosion and Coatings
Differential thermal analysis
Electron microscopy
Emission analysis
Engineering
Glass
Heat treating
Heat treatment
Intermetallic compounds
Investigations
Materials Science
Mechanical alloying
Melting point
Melting points
Metallic Materials
Metallurgy
Nanocomposites
Natural Materials
Nickel oxides
Particle size
Scanning electron microscopy
Surfaces and Interfaces
Temperature
Thermal analysis
Thin Films
Titanium dioxide
Transmission electron microscopy
Tribology
X-ray diffraction
title Synthesis of a NiTi2-AlNi-Al2O3 nanocomposite by mechanical alloying and heat treatment of Al-TiO2-NiO
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