Fe3O4@MCM-48–SO3H： An efficient magnetically separable nanocatalyst for the synthesis of benzo[f]chromeno[2,3-d]pyrimidinones

Sulfonic acid groups were grafted onto three different types of synthesized magnetic nanoparticles, namely Fe3O4, Fe3O4@SiO2, and Fe3O4@MCM-48. The sulfonic acid-functionalized nanoparticles were evaluated as catalysts for the synthesis of 5-aryl-1H-benzo[f]chromeno[2,3-d]pyrimidine-2,4（3H,5H）-dione...

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Published in:Chinese journal of catalysis 2015-04, Vol.36 (4), p.572-578
Main Authors: Kefayati, Hassan, Golshekan, Mostafa, Shariati, Shahab, Bagheri, Mahsa
Format: Article
Language:English
Subjects:
Benzo[f]chromene
Chromeno[2,3-d] pyrimidine
Fe3O4
Fe3O4@MCM-48–SO3H
Fe3O4@SiO2–SO3H
MCM-48
Mesoporous magnetic nanoparticle
分离
合成
嘧啶酮
均相催化剂
磁性纳米颗粒
纳米催化剂
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cited_by cdi_FETCH-LOGICAL-c417t-3d6f67d4ffd2f1f5c7b6f353c9c9da7f148f77156e3abe705ddb6972c03f1b703
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container_title Chinese journal of catalysis
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creator Kefayati, Hassan
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description Sulfonic acid groups were grafted onto three different types of synthesized magnetic nanoparticles, namely Fe3O4, Fe3O4@SiO2, and Fe3O4@MCM-48. The sulfonic acid-functionalized nanoparticles were evaluated as catalysts for the synthesis of 5-aryl-1H-benzo[f]chromeno[2,3-d]pyrimidine-2,4（3H,5H）-dione derivatives in terms of activity and recyclability. Their catalytic activities were compared with that of the homogeneous acid catalyst 1-methylimidazolium hydrogen sulfate（[HMIm][HSO4]）. The activity of Fe3O4@MCM-48–SO3H was comparable to those of the other heter-ogeneous and homogeneous catalysts.
doi_str_mv 10.1016/S1872-2067(14)60286-2
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subjects Benzo[f]chromene
Chromeno[2,3-d] pyrimidine
Fe3O4
Fe3O4@MCM-48–SO3H
Fe3O4@SiO2–SO3H
MCM-48
Mesoporous magnetic nanoparticle
分离
合成
嘧啶酮
均相催化剂
磁性纳米颗粒
纳米催化剂
title Fe3O4@MCM-48–SO3H： An efficient magnetically separable nanocatalyst for the synthesis of benzo[f]chromeno[2,3-d]pyrimidinones
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