Intermolecular cyclocondensation reaction of 3,4-dihydropyrimidine-2-thione under the Mitsunobu reaction conditions

A self-intermolecular cyclocondensation reaction of 3,4-dihydropyrimidine-2-thione（DHPM） to give a novel tricyclic structure containing DHPM core in the presence of diethyl azodicarboxylate（DEAD） and triphenylphosphine（TPP） at room temperature is reported.

Saved in:
Bibliographic Details
Published in:Chinese chemical letters 2011-06, Vol.22 (6), p.679-682
Main Authors: Da, Yu Xia, Zhang, Zhang, Quan, Zheng Jun
Format: Article
Language:English
Subjects:
3,4-Dihydropyrimidine-2-thiones
Cyclocondensation
Mitsunobu reaction
TPP
三环结构
三苯基膦
二氢
分子间
反应条件
嘧啶
硫酮
Citations: Items that this one cites
Items that cite this one
Online Access:Get full text
Tags: Add Tag
No Tags, Be the first to tag this record!
Description
Summary:A self-intermolecular cyclocondensation reaction of 3,4-dihydropyrimidine-2-thione（DHPM） to give a novel tricyclic structure containing DHPM core in the presence of diethyl azodicarboxylate（DEAD） and triphenylphosphine（TPP） at room temperature is reported.
ISSN:1001-8417
1878-5964
DOI:10.1016/j.cclet.2010.12.041