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Porous graphene decorated silica as a new stationary phase for separation of sulfanilamide compounds in hydrophilic interaction chromatography
Porous graphene (PG) was prepared by combustion method and then coated onto aminopropyl-silica in deep eutectic solven nb ts (DESs). PG-modified silica was evaluated in hydrophilic interaction chromatography for the separation and determination of sulfonamides in human serum samples. [Display omitte...
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Published in: | Chinese chemical letters 2019-04, Vol.30 (4), p.863-866 |
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creator | Song, Lijun Zhang, Haijuan Cai, Tianpei Chen, Jia Li, Zhan Guan, Ming Qiu, Hongdeng |
description | Porous graphene (PG) was prepared by combustion method and then coated onto aminopropyl-silica in deep eutectic solven nb ts (DESs). PG-modified silica was evaluated in hydrophilic interaction chromatography for the separation and determination of sulfonamides in human serum samples.
[Display omitted]
Porous graphene (PG) has potential applications in numerous fields because of the existence of nanopores in the plane. In this study, porous graphene decorated silica microspheres (Sil-PG) were successfully fabricated by assembling PG onto the silica particles surface in deep eutectic solvents (DESs). Experimental results demonstrate that this new stationary phase can facilitate the separation of six sulfonamides compounds in hydrophilic chromatographic conditions. The successful synthesis of the Sil-PG stationary phase provides a basis for the application of porous graphene-modified materials as the stationary phase for liquid chromatography, and offers the possibility to broaden the application of PG in the field of chromatography. |
doi_str_mv | 10.1016/j.cclet.2018.10.040 |
format | article |
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[Display omitted]
Porous graphene (PG) has potential applications in numerous fields because of the existence of nanopores in the plane. In this study, porous graphene decorated silica microspheres (Sil-PG) were successfully fabricated by assembling PG onto the silica particles surface in deep eutectic solvents (DESs). Experimental results demonstrate that this new stationary phase can facilitate the separation of six sulfonamides compounds in hydrophilic chromatographic conditions. The successful synthesis of the Sil-PG stationary phase provides a basis for the application of porous graphene-modified materials as the stationary phase for liquid chromatography, and offers the possibility to broaden the application of PG in the field of chromatography.</description><identifier>ISSN: 1001-8417</identifier><identifier>EISSN: 1878-5964</identifier><identifier>DOI: 10.1016/j.cclet.2018.10.040</identifier><language>eng</language><publisher>Elsevier B.V</publisher><subject>Human serum samples ; Hydrophilic interaction chromatography ; Porous graphene ; Stationary phase ; Sulfonamides</subject><ispartof>Chinese chemical letters, 2019-04, Vol.30 (4), p.863-866</ispartof><rights>2019 The Author</rights><rights>Copyright © Wanfang Data Co. Ltd. All Rights Reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c401t-df80c078b7764917cc5da08f37d6a7bf48dbe9abf51ad050c6fcfe325b7c2ae43</citedby><cites>FETCH-LOGICAL-c401t-df80c078b7764917cc5da08f37d6a7bf48dbe9abf51ad050c6fcfe325b7c2ae43</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Uhttp://www.wanfangdata.com.cn/images/PeriodicalImages/zghxkb/zghxkb.jpg</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids></links><search><creatorcontrib>Song, Lijun</creatorcontrib><creatorcontrib>Zhang, Haijuan</creatorcontrib><creatorcontrib>Cai, Tianpei</creatorcontrib><creatorcontrib>Chen, Jia</creatorcontrib><creatorcontrib>Li, Zhan</creatorcontrib><creatorcontrib>Guan, Ming</creatorcontrib><creatorcontrib>Qiu, Hongdeng</creatorcontrib><title>Porous graphene decorated silica as a new stationary phase for separation of sulfanilamide compounds in hydrophilic interaction chromatography</title><title>Chinese chemical letters</title><description>Porous graphene (PG) was prepared by combustion method and then coated onto aminopropyl-silica in deep eutectic solven nb ts (DESs). PG-modified silica was evaluated in hydrophilic interaction chromatography for the separation and determination of sulfonamides in human serum samples.
[Display omitted]
Porous graphene (PG) has potential applications in numerous fields because of the existence of nanopores in the plane. In this study, porous graphene decorated silica microspheres (Sil-PG) were successfully fabricated by assembling PG onto the silica particles surface in deep eutectic solvents (DESs). Experimental results demonstrate that this new stationary phase can facilitate the separation of six sulfonamides compounds in hydrophilic chromatographic conditions. The successful synthesis of the Sil-PG stationary phase provides a basis for the application of porous graphene-modified materials as the stationary phase for liquid chromatography, and offers the possibility to broaden the application of PG in the field of chromatography.</description><subject>Human serum samples</subject><subject>Hydrophilic interaction chromatography</subject><subject>Porous graphene</subject><subject>Stationary phase</subject><subject>Sulfonamides</subject><issn>1001-8417</issn><issn>1878-5964</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><recordid>eNp9kM9uEzEQh1cIJErLE_TiG6cN4-wfOwcOqIKCVAkO9GzNjsdZh429sjeU9CF4ZpyEMyfbP803M_6q6lbCSoLs3-9WRBMvqzVIXZIVtPCiupJa6brb9O3LcgeQtW6lel29yXkHsNa66a-qP99jiocstgnnkQMLyxQTLmxF9pMnFJgFisBPIi-4-BgwHcU8YmbhYhKZZ0znXEQn8mFyGPyEe29ZUNzP8RBsFj6I8WhTnMdTz_JcOCGdKRpT3OMSzwscb6pXDqfMb_-d19Xj508_7r7UD9_uv959fKipBbnU1mkgUHpQqm83UhF1FkG7Rtke1eBabQfe4OA6iRY6oN6R42bdDYrWyG1zXb279H3CUDbeml08pFAmmuft-PvnUERuikRQpbK5VFKKOSd2Zk5-XyQYCeYk3-zMWb45yT-FhSvUhwvF5RO_PCeTyXMgtj4xLcZG_1_-L3Rnk80</recordid><startdate>20190401</startdate><enddate>20190401</enddate><creator>Song, Lijun</creator><creator>Zhang, Haijuan</creator><creator>Cai, Tianpei</creator><creator>Chen, Jia</creator><creator>Li, Zhan</creator><creator>Guan, Ming</creator><creator>Qiu, Hongdeng</creator><general>Elsevier B.V</general><general>Laboratory on Pollution Monitoring and Control, College of Chemistry and Chemical Engineering, Xinjiang Normal University, Urumqi 830054, China</general><general>CAS Key Laboratory of Chemistry of Northwestern Plant Resources and Key Laboratory for Natural Medicine of Gansu Province, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, China%CAS Key Laboratory of Chemistry of Northwestern Plant Resources and Key Laboratory for Natural Medicine of Gansu Province, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, China%Laboratory on Pollution Monitoring and Control, College of Chemistry and Chemical Engineering, Xinjiang Normal University, Urumqi 830054, China</general><scope>AAYXX</scope><scope>CITATION</scope><scope>2B.</scope><scope>4A8</scope><scope>92I</scope><scope>93N</scope><scope>PSX</scope><scope>TCJ</scope></search><sort><creationdate>20190401</creationdate><title>Porous graphene decorated silica as a new stationary phase for separation of sulfanilamide compounds in hydrophilic interaction chromatography</title><author>Song, Lijun ; Zhang, Haijuan ; Cai, Tianpei ; Chen, Jia ; Li, Zhan ; Guan, Ming ; Qiu, Hongdeng</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c401t-df80c078b7764917cc5da08f37d6a7bf48dbe9abf51ad050c6fcfe325b7c2ae43</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2019</creationdate><topic>Human serum samples</topic><topic>Hydrophilic interaction chromatography</topic><topic>Porous graphene</topic><topic>Stationary phase</topic><topic>Sulfonamides</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Song, Lijun</creatorcontrib><creatorcontrib>Zhang, Haijuan</creatorcontrib><creatorcontrib>Cai, Tianpei</creatorcontrib><creatorcontrib>Chen, Jia</creatorcontrib><creatorcontrib>Li, Zhan</creatorcontrib><creatorcontrib>Guan, Ming</creatorcontrib><creatorcontrib>Qiu, Hongdeng</creatorcontrib><collection>CrossRef</collection><collection>Wanfang Data Journals - Hong Kong</collection><collection>WANFANG Data Centre</collection><collection>Wanfang Data Journals</collection><collection>万方数据期刊 - 香港版</collection><collection>China Online Journals (COJ)</collection><collection>China Online Journals (COJ)</collection><jtitle>Chinese chemical letters</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Song, Lijun</au><au>Zhang, Haijuan</au><au>Cai, Tianpei</au><au>Chen, Jia</au><au>Li, Zhan</au><au>Guan, Ming</au><au>Qiu, Hongdeng</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Porous graphene decorated silica as a new stationary phase for separation of sulfanilamide compounds in hydrophilic interaction chromatography</atitle><jtitle>Chinese chemical letters</jtitle><date>2019-04-01</date><risdate>2019</risdate><volume>30</volume><issue>4</issue><spage>863</spage><epage>866</epage><pages>863-866</pages><issn>1001-8417</issn><eissn>1878-5964</eissn><abstract>Porous graphene (PG) was prepared by combustion method and then coated onto aminopropyl-silica in deep eutectic solven nb ts (DESs). PG-modified silica was evaluated in hydrophilic interaction chromatography for the separation and determination of sulfonamides in human serum samples.
[Display omitted]
Porous graphene (PG) has potential applications in numerous fields because of the existence of nanopores in the plane. In this study, porous graphene decorated silica microspheres (Sil-PG) were successfully fabricated by assembling PG onto the silica particles surface in deep eutectic solvents (DESs). Experimental results demonstrate that this new stationary phase can facilitate the separation of six sulfonamides compounds in hydrophilic chromatographic conditions. The successful synthesis of the Sil-PG stationary phase provides a basis for the application of porous graphene-modified materials as the stationary phase for liquid chromatography, and offers the possibility to broaden the application of PG in the field of chromatography.</abstract><pub>Elsevier B.V</pub><doi>10.1016/j.cclet.2018.10.040</doi><tpages>4</tpages></addata></record> |
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ispartof | Chinese chemical letters, 2019-04, Vol.30 (4), p.863-866 |
issn | 1001-8417 1878-5964 |
language | eng |
recordid | cdi_wanfang_journals_zghxkb201904007 |
source | Elsevier |
subjects | Human serum samples Hydrophilic interaction chromatography Porous graphene Stationary phase Sulfonamides |
title | Porous graphene decorated silica as a new stationary phase for separation of sulfanilamide compounds in hydrophilic interaction chromatography |
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