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Synthesis, Properties, and Evolution Mechanism of Morphology Tunable InPO4 Crystals
In the synthesis of InPO4 crystals, using F127 [(EO)106(PO)70(EO)106] as a structure‐directing template, a morphology tunable progress was observed during the crystal evolution. By verifying the initial pH from 1.0 to 12.0, the morphology is evolved from single crystal, through sub‐micro crystallite...
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Published in: | Journal of the Chinese Chemical Society (Taipei) 2007-10, Vol.54 (5), p.1123-1128 |
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container_title | Journal of the Chinese Chemical Society (Taipei) |
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creator | Lin, Xin-Hong Wang, Ya-Chen Su, Yu-Han Yang, Chung-Sung |
description | In the synthesis of InPO4 crystals, using F127 [(EO)106(PO)70(EO)106] as a structure‐directing template, a morphology tunable progress was observed during the crystal evolution. By verifying the initial pH from 1.0 to 12.0, the morphology is evolved from single crystal, through sub‐micro crystallites, and finally to crystalline nanoparticles. The most influential factors in the morphology evolution are the initial pH level, the participation of surfactant‐template F127, and the change in pH during the reaction. |
doi_str_mv | 10.1002/jccs.200700161 |
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By verifying the initial pH from 1.0 to 12.0, the morphology is evolved from single crystal, through sub‐micro crystallites, and finally to crystalline nanoparticles. The most influential factors in the morphology evolution are the initial pH level, the participation of surfactant‐template F127, and the change in pH during the reaction.</description><subject>Crystallization</subject><subject>InPO4</subject><subject>Single crystal</subject><subject>X-ray diffraction (XRD)</subject><issn>0009-4536</issn><issn>2192-6549</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2007</creationdate><recordtype>article</recordtype><recordid>eNo9kF1PwjAUhhujiYjeet0f4PC0Xct6acaHEBCSYbxsSlekODbSDnX_3hEMV-95L56TNw9CjwR6BIA-74wJPQrQByCCXKEOJZJGgsfyGnUAQEYxZ-IW3YWwA4gZ5bKDsqwp660NLjzhpa8O1tfOtrcuczz8ropj7aoSz63Z6tKFPa42eF75w7Yqqs8Gr46lXhcWT8rlIsapb0Kti3CPbjZt2If_7KL30XCVvkazxXiSvswiR2NGooTkhCaM85wlViewWRspDZDcCs1oLHQ7nzMqklzyNbUkN7mlDISwCTdUAusief774wrbqIN3e-0bRUCdfKiTD3XxoaZpml1ay0Zn1oXa_l5Y7b-U6LM-Vx9vY0UHhInBlKgR-wNhmmUm</recordid><startdate>200710</startdate><enddate>200710</enddate><creator>Lin, Xin-Hong</creator><creator>Wang, Ya-Chen</creator><creator>Su, Yu-Han</creator><creator>Yang, Chung-Sung</creator><general>WILEY-VCH Verlag</general><general>WILEY‐VCH Verlag</general><scope>BSCLL</scope></search><sort><creationdate>200710</creationdate><title>Synthesis, Properties, and Evolution Mechanism of Morphology Tunable InPO4 Crystals</title><author>Lin, Xin-Hong ; Wang, Ya-Chen ; Su, Yu-Han ; Yang, Chung-Sung</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-i2431-81d128355d38ea80fbc99c01de6a3246a19253268d95b2e1dcde23066e85c2903</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2007</creationdate><topic>Crystallization</topic><topic>InPO4</topic><topic>Single crystal</topic><topic>X-ray diffraction (XRD)</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Lin, Xin-Hong</creatorcontrib><creatorcontrib>Wang, Ya-Chen</creatorcontrib><creatorcontrib>Su, Yu-Han</creatorcontrib><creatorcontrib>Yang, Chung-Sung</creatorcontrib><collection>Istex</collection><jtitle>Journal of the Chinese Chemical Society (Taipei)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Lin, Xin-Hong</au><au>Wang, Ya-Chen</au><au>Su, Yu-Han</au><au>Yang, Chung-Sung</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis, Properties, and Evolution Mechanism of Morphology Tunable InPO4 Crystals</atitle><jtitle>Journal of the Chinese Chemical Society (Taipei)</jtitle><addtitle>Jnl Chinese Chemical Soc</addtitle><date>2007-10</date><risdate>2007</risdate><volume>54</volume><issue>5</issue><spage>1123</spage><epage>1128</epage><pages>1123-1128</pages><issn>0009-4536</issn><eissn>2192-6549</eissn><abstract>In the synthesis of InPO4 crystals, using F127 [(EO)106(PO)70(EO)106] as a structure‐directing template, a morphology tunable progress was observed during the crystal evolution. By verifying the initial pH from 1.0 to 12.0, the morphology is evolved from single crystal, through sub‐micro crystallites, and finally to crystalline nanoparticles. The most influential factors in the morphology evolution are the initial pH level, the participation of surfactant‐template F127, and the change in pH during the reaction.</abstract><cop>Weinheim</cop><pub>WILEY-VCH Verlag</pub><doi>10.1002/jccs.200700161</doi><tpages>6</tpages></addata></record> |
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subjects | Crystallization InPO4 Single crystal X-ray diffraction (XRD) |
title | Synthesis, Properties, and Evolution Mechanism of Morphology Tunable InPO4 Crystals |
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