1H and 13C spectral assignment of naphtho[2′,1′:5,6]-naphtho[2′,1′:4,5]thieno[2,3-c]quinoline using the IDR-GHSQC-TOCSY experiment

The assignment of the NMR spectra of the polynuclear heteroaromatic naphtho[2′,1′:5,6]naphtho‐[2′,1′:4,5]thieno[2,3‐c]quinoline is reported. The analysis was based on the homonuclear ROESY, heteronuclear direct GHSQC, IDR‐GHSQC‐TOCSY, and long‐range GHMBC experiments. The complete 1H and 13C shift a...

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Bibliographic Details
Published in:Journal of heterocyclic chemistry 2000-07, Vol.37 (4), p.821-825
Main Authors: Hadden, Chad E., Martin, Gary E., Luo, J.-K., Castle, Raymond N.
Format: Article
Language:English
Online Access:Get full text
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Summary:The assignment of the NMR spectra of the polynuclear heteroaromatic naphtho[2′,1′:5,6]naphtho‐[2′,1′:4,5]thieno[2,3‐c]quinoline is reported. The analysis was based on the homonuclear ROESY, heteronuclear direct GHSQC, IDR‐GHSQC‐TOCSY, and long‐range GHMBC experiments. The complete 1H and 13C shift assignments are reported.
ISSN:0022-152X
1943-5193
DOI:10.1002/jhet.5570370425