Creep behavior of Nextel™720/alumina–mullite ceramic composite with ±45° fiber orientation at 1200 °C

• Published in: Materials science & engineering. A, Structural materials : properties, microstructure and processing Structural materials : properties, microstructure and processing, 2010, Vol.527 (20), p.5326-5334
• Main Authors: Ruggles-Wrenn, M.B., Ozer, M.
• Format: Article
• Language: English
• Subjects: Ceramic-matrix composites (CMCs); Condensed matter: structure, mechanical and thermal properties; Creep; Elasticity, elastic constants; Exact sciences and technology; Fractography; High-temperature properties; Mechanical and acoustical properties of condensed matter; Mechanical properties of solids; Oxides; Physics
• ISSN: 0921-5093; 1873-4936
• DOI: 10.1016/j.msea.2010.05.030

The tensile creep behavior of an oxide–oxide continuous fiber ceramic composite with ±45° fiber orientation was investigated at 1200 °C in laboratory air, in steam and in argon. The composite consists of a porous alumina–mullite matrix reinforced with laminated, woven mullite/alumina (Nextel™720) fibers, has no interface between the fiber and matrix, and relies on the porous matrix for flaw tolerance. The tensile stress–strain behavior was investigated and the tensile properties measured at 1200 °C. The elastic modulus was 38.6 GPa and the ultimate tensile strength (UTS) was 37 MPa. Tensile creep behavior was examined for creep stresses in the 13–32 MPa range. Primary and secondary creep regimes were observed in all tests. Creep run-out (set to 100 h) was achieved in all test environments for creep stress levels ≤20 MPa. At creep stresses >20 MPa, creep performance was best in laboratory air and worst in steam. The presence of either steam or argon accelerated creep rates and significantly reduced creep life. Composite microstructure, as well as damage and failure mechanisms were investigated. Matrix degradation appears to be the cause of early failures in argon and in steam.