Effect of sintering temperature on the properties of titanium matrix composites reinforced with Al0·5CoCrFeNi high-entropy alloy particles

• Published in: Materials science & engineering. A, Structural materials : properties, microstructure and processing Structural materials : properties, microstructure and processing, 2024-09, Vol.911, p.146920, Article 146920
• Main Authors: Yuan, Zhanwei, Wang, Kai, Li, Shurong, Jin, Xixin, Yu, Yuan, Guo, Min
• Format: Article
• Language: English
• Subjects: Discharge plasma sintering; Mechanical properties; Sintering mechanism; Strengthening mechanism; Titanium matrix composites
• ISSN: 0921-5093
• DOI: 10.1016/j.msea.2024.146920

In this study, the organization and mechanical properties of the composites were analyzed at different sintering temperatures, and it was found that the local high-temperature phenomenon of discharge plasma sintering led to rapid melting and element diffusion at the junction of the high-entropy alloy particles and the Ti matrix, resulting in the formation of the interfacial layer. The increase in sintering temperature promoted close bonding between particles and element diffusion, caused lattice distortion and new phase formation, and increased the thickness of the interface layer and precipitated phase at the grain boundary. Most of the high-entropy alloy particles were dissolved when the sintering temperature reached 1050 °C. The composites were characterized by a high sintering temperature. The comprehensive mechanical properties of the composites first increased and then decreased when the sintering temperature increased, and they were optimized at 850 °C. The nanoindentation results show that the increase in sintering temperature leads to a decrease in the hardness of the high-entropy alloy particles, an increase in the hardness of the titanium matrix, and a higher hardness of the interfacial layer than that of the high-entropy alloy particles and the titanium matrix.