Copper-catalyzed C–N bond formation using dialkyl azodicarboxylate as the amination reagent

[Display omitted] An efficient copper-catalyzed reaction for C–N bond formation using aryl halides, dialkyl azodicarboxylate, and a hydride source is reported. Using this procedure, aryl iodides reacted at ambient conditions, while aryl bromides required heating to 60°C to accomplish the transformat...

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Bibliographic Details
Published in:Tetrahedron letters 2016-01, Vol.57 (4), p.463-465
Main Author: Samzadeh-Kermani, Alireza
Format: Article
Language:English
Subjects:
Aryl hydrazide
Copper salts
C–N cross-coupling
Dialkyl azodicarboxylate
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Summary:[Display omitted] An efficient copper-catalyzed reaction for C–N bond formation using aryl halides, dialkyl azodicarboxylate, and a hydride source is reported. Using this procedure, aryl iodides reacted at ambient conditions, while aryl bromides required heating to 60°C to accomplish the transformation. Various functional groups were tolerated under the optimum conditions.
ISSN:0040-4039
1873-3581
DOI:10.1016/j.tetlet.2015.12.036