Volatile compounds, sensory quality and ice morphology in falling-film and block freeze concentration of coffee extract

• Published in: Journal of food engineering 2015-12, Vol.166, p.64-71
• Main Authors: Moreno, F.L., Quintanilla-Carvajal, M.X., Sotelo, L.I., Osorio, C., Raventós, M., Hernández, E., Ruiz, Y.
• Format: Article
• Language: English
• Subjects: Anàlisi sensorial; Begudes; Cafè; Coffee; Coffee concentration; Composition; Cryoconcentration; Enginyeria agroalimentària; Ice morphology; Indústries agroalimentàries; Sensory evaluation; Volatiles; Volatiles Cryoconcentration; Àrees temàtiques de la UPC
• ISSN: 0260-8774; 1873-5770
• DOI: 10.1016/j.jfoodeng.2015.05.018

•Block and falling film freeze concentration of coffee extract were compared.•The major volatile compounds of the coffee extracts were preserved.•The sensory attributes of the freeze-concentrated extract were preserved.•Falling film technique produced high solute occlusion and small ice crystals.•The dewatering capacity was higher for the falling-film technique. Coffee extract was freeze-concentrated through block and falling-film techniques. Solute retention and concentration efficiency were determined after one stage of these processes. Ice morphology was characterized through image analysis. Preservation of volatile compounds was determined through GC–MS. The effect of coffee extract on flavour was determined after freeze concentration through sensory evaluation. Solute occlusion was higher for falling-film than for block freeze-concentration, with an average distribution coefficient of 0.45 and 0.29, respectively. The ice crystal size was lower for the falling-film technique; this explains the higher solute occlusion. The dewatering capacity was higher for the falling-film technique, as this process is faster than block freeze-concentration. The most abundant volatile compounds of the coffee extracts were preserved after freeze concentration with both techniques. In the same way, no differences were found in most of the sensory attributes of the freeze-concentrated extract obtained using both techniques. Our results confirm the benefits of the block and falling-film freeze concentration techniques in preserving the quality of coffee extracts.