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A new look at NaBrF4: the most BrF3-rich tetrafluoridobromate(III) by mass
Sodium tetrafluoridobromate(III) was synthesized and characterized. The compound crystallizes isotypic to potassium and rubidium tetrafluoridobromate(III) in the tetragonal space group type I 4/ mcm with a = 5.7239(8) Å, c = 10.331(2) Å, V = 338.47(12) Å 3 , and Z = 4 at T = 110 K. Also, the co...
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| Published in: | Monatshefte für Chemie 2016-10, Vol.147 (10), p.1661-1668 |
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| creator | Ivlev, Sergei I. Ostvald, Roman V. Kraus, Florian |
| description | Sodium tetrafluoridobromate(III) was synthesized and characterized. The compound crystallizes isotypic to potassium and rubidium tetrafluoridobromate(III) in the tetragonal space group type
I
4/
mcm
with
a
= 5.7239(8) Å,
c
= 10.331(2) Å,
V
= 338.47(12) Å
3
, and
Z
= 4 at
T
= 110 K. Also, the compound was investigated by means of powder X-ray diffraction, IR and Raman spectroscopy, and theoretical calculations.
Graphical abstract |
| doi_str_mv | 10.1007/s00706-016-1799-2 |
| format | article |
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I
4/
mcm
with
a
= 5.7239(8) Å,
c
= 10.331(2) Å,
V
= 338.47(12) Å
3
, and
Z
= 4 at
T
= 110 K. Also, the compound was investigated by means of powder X-ray diffraction, IR and Raman spectroscopy, and theoretical calculations.
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I
4/
mcm
with
a
= 5.7239(8) Å,
c
= 10.331(2) Å,
V
= 338.47(12) Å
3
, and
Z
= 4 at
T
= 110 K. Also, the compound was investigated by means of powder X-ray diffraction, IR and Raman spectroscopy, and theoretical calculations.
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I
4/
mcm
with
a
= 5.7239(8) Å,
c
= 10.331(2) Å,
V
= 338.47(12) Å
3
, and
Z
= 4 at
T
= 110 K. Also, the compound was investigated by means of powder X-ray diffraction, IR and Raman spectroscopy, and theoretical calculations.
Graphical abstract</abstract><cop>Vienna</cop><pub>Springer Vienna</pub><doi>10.1007/s00706-016-1799-2</doi><tpages>8</tpages></addata></record> |
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| identifier | ISSN: 0026-9247 |
| ispartof | Monatshefte für Chemie, 2016-10, Vol.147 (10), p.1661-1668 |
| issn | 0026-9247 1434-4475 |
| language | eng |
| recordid | cdi_proquest_journals_1880868047 |
| source | Springer Nature |
| subjects | Analytical Chemistry Chemistry Chemistry and Materials Science Chemistry/Food Science Infrared spectroscopy Inorganic Chemistry Organic Chemistry Original Paper Physical Chemistry Raman spectroscopy Rubidium Theoretical and Computational Chemistry X ray powder diffraction |
| title | A new look at NaBrF4: the most BrF3-rich tetrafluoridobromate(III) by mass |
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