An Improved Synthesis of Bromotetrazole

A new efficient synthesis of 5‐bromotetrazole is presented. The free acid bromotetrazole was synthesized in a straightforward reaction analogous to the production of nitrotetrazole. Its sodium salt was readily produced via acid/base salt metathesis. Both products were characterized chemically and as...

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Bibliographic Details
Published in:Zeitschrift für anorganische und allgemeine Chemie (1950) 2022-01, Vol.648 (2), p.n/a
Main Authors: Wozniak, Dominique R., Zeller, Matthias, Byrd, Edward C., Piercey, Davin G.
Format: Article
Language:English
Subjects:
Crystallography
Energetic materials
Heterocycles
Improved synthesis
Mass spectrometry
Metathesis
NMR
Nuclear magnetic resonance
Sodium salts
Tetrazoles
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Summary:A new efficient synthesis of 5‐bromotetrazole is presented. The free acid bromotetrazole was synthesized in a straightforward reaction analogous to the production of nitrotetrazole. Its sodium salt was readily produced via acid/base salt metathesis. Both products were characterized chemically and as energetic materials by 1H and 13C NMR, IR, High Resolution Mass Spectrometry, x‐ray crystallography, TGA, impact and friction tests.
ISSN:0044-2313
1521-3749
DOI:10.1002/zaac.202100333