Pd-catalyzed exclusively regioselective [5 + 4] cycloaddition for the construction of 1,5-di/ox-azonanes

An efficient approach for the construction of 1,5-di/ox-azonanes via Pd-catalyzed [5 + 4] cycloaddition has been developed. This reaction could tolerate a variety of functional groups with exclusive regioselectivity, affording a series of nine-membered heterocycles in moderate to excellent yields. T...

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Published in:Organic chemistry frontiers an international journal of organic chemistry 2023-03, Vol.10 (7), p.1680-1685
Main Authors: Liu, Wenqi, Zang, Meng, Zhang, Jian, Wang, Quannan, Yang-Zi, Liu, Wei-Ping, Deng
Format: Article
Language:English
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Cycloaddition
Functional groups
Organic chemistry
Palladium
Regioselectivity
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container_title Organic chemistry frontiers an international journal of organic chemistry
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creator Liu, Wenqi
Zang, Meng
Zhang, Jian
Wang, Quannan
Yang-Zi, Liu
Wei-Ping, Deng
description An efficient approach for the construction of 1,5-di/ox-azonanes via Pd-catalyzed [5 + 4] cycloaddition has been developed. This reaction could tolerate a variety of functional groups with exclusive regioselectivity, affording a series of nine-membered heterocycles in moderate to excellent yields. The synthetic utility of the current method was also demonstrated by a gram-scale reaction.
doi_str_mv 10.1039/d3qo00070b
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subjects Cycloaddition
Functional groups
Organic chemistry
Palladium
Regioselectivity
title Pd-catalyzed exclusively regioselective [5 + 4] cycloaddition for the construction of 1,5-di/ox-azonanes
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