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Synthesis of Nickel Oxide Nanoparticles from Thermal Decomposition of a New Precursor
Nickel oxide nanoparticles (25 nm) have been synthesized via decomposition of a new precursor nickel octanoate Ni(octa) 2 in the presence of oleylamine (C 18 H 37 N) and triphenylphosphine (C 18 H 15 P), in mild conditions. To control the particle size and morphology, combination of C 18 H 15 P and...
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| Published in: | Journal of cluster science 2012-06, Vol.23 (2), p.577-583 |
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| Main Authors: | , , , , |
| Format: | Article |
| Language: | English |
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| cited_by | cdi_FETCH-LOGICAL-c382t-61bb28d7ed3ea3337a8c986014c335eabb5e6788ab55fcef568f2702def080ce3 |
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| cites | cdi_FETCH-LOGICAL-c382t-61bb28d7ed3ea3337a8c986014c335eabb5e6788ab55fcef568f2702def080ce3 |
| container_end_page | 583 |
| container_issue | 2 |
| container_start_page | 577 |
| container_title | Journal of cluster science |
| container_volume | 23 |
| creator | Fereshteh, Zeinab Salavati-Niasari, Masoud Saberyan, Kamal Hosseinpour-Mashkani, S. Mostafa Tavakoli, Farnosh |
| description | Nickel oxide nanoparticles (25 nm) have been synthesized via decomposition of a new precursor nickel octanoate Ni(octa)
2
in the presence of oleylamine (C
18
H
37
N) and triphenylphosphine (C
18
H
15
P), in mild conditions. To control the particle size and morphology, combination of C
18
H
15
P and C
18
H
37
N were applied as surfactants. In this process, oleylamine was used as both the medium and the stabilizing reagent. C
18
H
37
N and C
18
H
15
P play an important role in preventing aggregation of NiO nanoparticles. The products were characterized by XRD, SEM, TEM, FT–IR, and TGA. |
| doi_str_mv | 10.1007/s10876-012-0477-8 |
| format | article |
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2
in the presence of oleylamine (C
18
H
37
N) and triphenylphosphine (C
18
H
15
P), in mild conditions. To control the particle size and morphology, combination of C
18
H
15
P and C
18
H
37
N were applied as surfactants. In this process, oleylamine was used as both the medium and the stabilizing reagent. C
18
H
37
N and C
18
H
15
P play an important role in preventing aggregation of NiO nanoparticles. The products were characterized by XRD, SEM, TEM, FT–IR, and TGA.</description><identifier>ISSN: 1040-7278</identifier><identifier>EISSN: 1572-8862</identifier><identifier>DOI: 10.1007/s10876-012-0477-8</identifier><language>eng</language><publisher>Boston: Springer US</publisher><subject>Agglomeration ; Catalysis ; Chemistry ; Chemistry and Materials Science ; Clusters ; Decomposition ; Ethanol ; Fourier transforms ; Inorganic Chemistry ; Nanochemistry ; Nanoparticles ; Nickel ; Nickel oxides ; Original Paper ; Particle size ; Physical Chemistry ; Precursors ; Reagents ; Scanning electron microscopy ; Surfactants ; Thermal decomposition ; Transmission electron microscopy</subject><ispartof>Journal of cluster science, 2012-06, Vol.23 (2), p.577-583</ispartof><rights>Springer Science+Business Media, LLC 2012</rights><rights>Springer Science+Business Media, LLC 2012.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c382t-61bb28d7ed3ea3337a8c986014c335eabb5e6788ab55fcef568f2702def080ce3</citedby><cites>FETCH-LOGICAL-c382t-61bb28d7ed3ea3337a8c986014c335eabb5e6788ab55fcef568f2702def080ce3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27923,27924</link.rule.ids></links><search><creatorcontrib>Fereshteh, Zeinab</creatorcontrib><creatorcontrib>Salavati-Niasari, Masoud</creatorcontrib><creatorcontrib>Saberyan, Kamal</creatorcontrib><creatorcontrib>Hosseinpour-Mashkani, S. Mostafa</creatorcontrib><creatorcontrib>Tavakoli, Farnosh</creatorcontrib><title>Synthesis of Nickel Oxide Nanoparticles from Thermal Decomposition of a New Precursor</title><title>Journal of cluster science</title><addtitle>J Clust Sci</addtitle><description>Nickel oxide nanoparticles (25 nm) have been synthesized via decomposition of a new precursor nickel octanoate Ni(octa)
2
in the presence of oleylamine (C
18
H
37
N) and triphenylphosphine (C
18
H
15
P), in mild conditions. To control the particle size and morphology, combination of C
18
H
15
P and C
18
H
37
N were applied as surfactants. In this process, oleylamine was used as both the medium and the stabilizing reagent. C
18
H
37
N and C
18
H
15
P play an important role in preventing aggregation of NiO nanoparticles. The products were characterized by XRD, SEM, TEM, FT–IR, and TGA.</description><subject>Agglomeration</subject><subject>Catalysis</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Clusters</subject><subject>Decomposition</subject><subject>Ethanol</subject><subject>Fourier transforms</subject><subject>Inorganic Chemistry</subject><subject>Nanochemistry</subject><subject>Nanoparticles</subject><subject>Nickel</subject><subject>Nickel oxides</subject><subject>Original Paper</subject><subject>Particle size</subject><subject>Physical Chemistry</subject><subject>Precursors</subject><subject>Reagents</subject><subject>Scanning electron microscopy</subject><subject>Surfactants</subject><subject>Thermal decomposition</subject><subject>Transmission electron microscopy</subject><issn>1040-7278</issn><issn>1572-8862</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><recordid>eNqFkc1LwzAYh4soOKd_gLeAFy_VfKzJu6PMTxib4HYOafrWdbbNTDp0_70ZFQRBPOU9PM8PwpMk54xeMUrVdWAUlEwp4ykdKZXCQTJgmeIpgOSH8aYjmiqu4Dg5CWFNKR2DEINk-bJruxWGKhBXklll37Am88-qQDIzrdsY31W2xkBK7xqyWKFvTE1u0bpm40LVVa7di4bM8IM8e7RbH5w_TY5KUwc8-36HyfL-bjF5TKfzh6fJzTS1AniXSpbnHAqFhUAjhFAG7BgkZSMrRIYmzzOUCsDkWVZaLDMJJVeUF1hSoBbFMLnsdzfevW8xdLqpgsW6Ni26bdCMcwaSjYD_j1LgkZZjGdGLX-jabX0bP6L5mAFXUjAWKdZT1rsQPJZ646vG-F2c0vsmum-iYxO9b6IhOrx3QmTbV_Q_y39LXwaTjiI</recordid><startdate>20120601</startdate><enddate>20120601</enddate><creator>Fereshteh, Zeinab</creator><creator>Salavati-Niasari, Masoud</creator><creator>Saberyan, Kamal</creator><creator>Hosseinpour-Mashkani, S. 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Mostafa ; Tavakoli, Farnosh</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c382t-61bb28d7ed3ea3337a8c986014c335eabb5e6788ab55fcef568f2702def080ce3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>Agglomeration</topic><topic>Catalysis</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Clusters</topic><topic>Decomposition</topic><topic>Ethanol</topic><topic>Fourier transforms</topic><topic>Inorganic Chemistry</topic><topic>Nanochemistry</topic><topic>Nanoparticles</topic><topic>Nickel</topic><topic>Nickel oxides</topic><topic>Original Paper</topic><topic>Particle size</topic><topic>Physical Chemistry</topic><topic>Precursors</topic><topic>Reagents</topic><topic>Scanning electron microscopy</topic><topic>Surfactants</topic><topic>Thermal decomposition</topic><topic>Transmission electron microscopy</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Fereshteh, Zeinab</creatorcontrib><creatorcontrib>Salavati-Niasari, Masoud</creatorcontrib><creatorcontrib>Saberyan, Kamal</creatorcontrib><creatorcontrib>Hosseinpour-Mashkani, S. 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Mostafa</au><au>Tavakoli, Farnosh</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of Nickel Oxide Nanoparticles from Thermal Decomposition of a New Precursor</atitle><jtitle>Journal of cluster science</jtitle><stitle>J Clust Sci</stitle><date>2012-06-01</date><risdate>2012</risdate><volume>23</volume><issue>2</issue><spage>577</spage><epage>583</epage><pages>577-583</pages><issn>1040-7278</issn><eissn>1572-8862</eissn><abstract>Nickel oxide nanoparticles (25 nm) have been synthesized via decomposition of a new precursor nickel octanoate Ni(octa)
2
in the presence of oleylamine (C
18
H
37
N) and triphenylphosphine (C
18
H
15
P), in mild conditions. To control the particle size and morphology, combination of C
18
H
15
P and C
18
H
37
N were applied as surfactants. In this process, oleylamine was used as both the medium and the stabilizing reagent. C
18
H
37
N and C
18
H
15
P play an important role in preventing aggregation of NiO nanoparticles. The products were characterized by XRD, SEM, TEM, FT–IR, and TGA.</abstract><cop>Boston</cop><pub>Springer US</pub><doi>10.1007/s10876-012-0477-8</doi><tpages>7</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1040-7278 |
| ispartof | Journal of cluster science, 2012-06, Vol.23 (2), p.577-583 |
| issn | 1040-7278 1572-8862 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_1221861482 |
| source | Springer Nature |
| subjects | Agglomeration Catalysis Chemistry Chemistry and Materials Science Clusters Decomposition Ethanol Fourier transforms Inorganic Chemistry Nanochemistry Nanoparticles Nickel Nickel oxides Original Paper Particle size Physical Chemistry Precursors Reagents Scanning electron microscopy Surfactants Thermal decomposition Transmission electron microscopy |
| title | Synthesis of Nickel Oxide Nanoparticles from Thermal Decomposition of a New Precursor |
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