In situ X-ray diffraction study of stacking fault formation in the near-surface region of transformation induced plasticity steels

• Published in: Thin solid films 2013-03, Vol.530, p.105-112
• Main Authors: Rafaja, David, Krbetschek, Christina, Borisova, Daria, Schreiber, Gerhard, Klemm, Volker
• Format: Article
• Language: English
• Subjects: Anisotropy; Austenite; Bending test; Composition and phase identification; Condensed matter: structure, mechanical and thermal properties; Crystal defects; Crystallographic anisotropy; Cubic lattice; Defects and impurities in crystals; microstructure; Defects and impurities: doping, implantation, distribution, concentration, etc; Diffraction; Exact sciences and technology; Lattice strain; Microstructure; Phase composition; Physics; Stacking faults; Stacking faults and other planar or extended defects; Structure and morphology; thickness; Structure of solids and liquids; crystallography; Surfaces and interfaces; thin films and whiskers (structure and nonelectronic properties); Thin film structure and morphology; Transmission electron microscopy; X-ray diffraction; X-rays
• ISSN: 0040-6090; 1879-2731
• DOI: 10.1016/j.tsf.2012.07.067

Formation of stacking faults in the near-surface region of Cr–Mn–Ni steels that shows the effect of transformation induced plasticity (TRIP) was investigated by means of in situ X-ray diffraction experiments during a tensile deformation of the samples up to approximately 9%. The X-ray diffraction measurements revealed simultaneously the phase transformation of the TRIP steel during its plastic deformation and the changes in the interplanar spacing of the diffraction lines of austenite. As the interplanar spacing in austenite is influenced both by the residual elastic lattice strain and by the stacking fault density, the crystallographic anisotropy of the cubic lattice parameter was employed to distinguish these effects. Despite a partial correlation between the cubic invariant, which describes the crystallographic anisotropy of the stress-induced lattice deformation, and the orientation factor of the stacking faults in austenite, which describes the effect of the stacking faults on the orientation-dependent shift of the X-ray diffraction lines, the crystallographic anisotropy of the lattice parameter of austenite was proven to be capable of tracking the formation of microstructure defects and of distinguishing individual microstructure defects from each other. The X-ray diffraction experiments were complemented by transmission electron microscopy, which allowed the different observed anisotropies of the cubic lattice parameter to be assigned to specific microstructure defects. ► Formation of stacking faults in TRIP steel was tracked by using X-ray diffraction. ► The key method was the analysis of the anisotropy of the cubic lattice parameter. ► Observed anisotropy results from interplay between elastic and plastic deformation. ► Validity of Warren's model is discussed in terms of the stacking fault arrangement.