Hydrothermal Synthesis and Size Control of Fe sub(3)O sub(4) Nanoparticles in the Presence of 2,2',2",2"'-(ethane-1,2-diylbis(azanetr iyl))tetraacetohydrazide

The synthesis and characterization of magnetite nanoparticles in the presence of 2,2',2 double prime ,2 double prime '-(ethane-1,2-diylbis(azanetr iyl)) tetraacetohydrazide as reducing agent in hydrothermal reaction were performed. Fe sub(3)O sub(4) nanoparticles with a diameter range 15-2...

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Bibliographic Details
Published in:Synthesis and reactivity in inorganic, metal-organic, and nano-metal chemistry metal-organic, and nano-metal chemistry, 2014-01, Vol.44 (8), p.1161-1165
Main Authors: Nemati, Ahlam, Shadpour, Sasan, Khalafbeygi, Hamid, Barkhi, Mohammad
Format: Article
Language:English
Subjects:
Ligands
Magnetite
Nanoparticles
Precursors
Reducing agents
Scanning electron microscopy
Synthesis
X-rays
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Summary:The synthesis and characterization of magnetite nanoparticles in the presence of 2,2',2 double prime ,2 double prime '-(ethane-1,2-diylbis(azanetr iyl)) tetraacetohydrazide as reducing agent in hydrothermal reaction were performed. Fe sub(3)O sub(4) nanoparticles with a diameter range 15-21 nm were achieved. The formation of pure Fe sub(3)O sub(4) nanoparticles was confirmed by XRD patterns and electron dispersive X-ray (EDX) analysis. The morphology of particles was characterized by scanning electron microscopy (SEM). The effects of reactants ratio, reducing agent and precursor, reaction temperature, and process time are described. It was found that the different reaction conditions such as ligand concentration, reaction temperature, and process time had little effect on the size of the synthesized nanoparticles.
ISSN:1553-3174
1553-3182
DOI:10.1080/15533174.2013.797443