Multi-class, multi-residue determination of 132 veterinary drugs in milk by magnetic solid-phase extraction based on magnetic hypercrosslinked polystyrene prior to their determination by high-performance liquid chromatography–tandem mass spectrometry

•A multi-class multi-residue analytical method for veterinary drugs was developed.•A total of 132 veterinary drugs from almost 15 classes were investigated.•A magnetic hypercrosslinked polystyrene-based MSPE was developed.•The methodology was applied to the trace drug analysis of milk. A quantitativ...

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Bibliographic Details
Published in:Food chemistry 2022-09, Vol.387, p.132866, Article 132866
Main Authors: Melekhin, A.O., Tolmacheva, V.V., Goncharov, N.O., Apyari, V.V., Dmitrienko, S.G., Shubina, E.G., Grudev, A.I.
Format: Article
Language:English
Subjects:
Animals
anthelmintics
Anti-Bacterial Agents - analysis
benzimidazoles
Benzimidazoles - analysis
beta-Lactams - analysis
Chromatography, High Pressure Liquid - methods
coccidiostats
Coccidiostats - analysis
crosslinking
Drug Residues - analysis
food chemistry
high performance liquid chromatography
HPLC-MS/MS
Lincosamides - analysis
macrolides
Macrolides - analysis
Magnetic hypercrosslinked polystyrene
Magnetic Phenomena
Magnetic solid-phase extraction
magnetism
Milk
Milk - chemistry
Multiclass analysis
multiresidue analysis
nitrofurans
Nitrofurans - analysis
nitroimidazoles
Nitroimidazoles - analysis
Polystyrenes
quinolones
Quinolones - analysis
Quinoxalines - analysis
Solid Phase Extraction
Sulfonamides - analysis
tandem mass spectrometry
Tandem Mass Spectrometry - methods
Tetracyclines - analysis
Veterinary drugs
Veterinary Drugs - analysis
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