Azobenzene-based unnatural amino acid scaffolds via a Pd( ii )-catalyzed C(sp 3 )–H arylation strategy

Azobenzene-based unnatural amino acid motifs were synthesized via Pd( ii )-catalyzed diastereoselective C(sp 3 )–H arylation of amino acid carboxamides with iodoacetanilides and Mills azo coupling.

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Bibliographic Details
Published in:Chemical communications (Cambridge, England) England), 2022-11, Vol.58 (93), p.12967-12970
Main Authors: Tomar, Radha, Suwasia, Sonam, Choudhury, Angshuman Roy, Venkataramani, Sugumar, Babu, Srinivasarao Arulananda
Format: Article
Language:English
Subjects:
Amino acids
Azo compounds
Chemical synthesis
Stereoselectivity
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Description
Summary:Azobenzene-based unnatural amino acid motifs were synthesized via Pd( ii )-catalyzed diastereoselective C(sp 3 )–H arylation of amino acid carboxamides with iodoacetanilides and Mills azo coupling.
ISSN:1359-7345
1364-548X
DOI:10.1039/d2cc04870a