Continuous Flow Synthesis of N,O‑Dimethyl‑N′‑nitroisourea Monitored by Inline Fourier Transform Infrared Spectroscopy: Bayesian Optimization and Kinetic Modeling

The synthesis of N,O-dimethyl-N′-nitroisourea, crucial intermediates in pesticide manufacturing, was explored through a substitution reaction between O-methyl-N-nitroisourea and methylamine within a novel continuous flow microreactor system, featuring Fourier transform infrared (FTIR) in-line analys...

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Bibliographic Details
Published in:Industrial & engineering chemistry research 2024-06, Vol.63 (23), p.10162-10171
Main Authors: Guo, Jiapeng, Luo, Guihua, Chai, Kejie, Su, Weike, Su, An
Format: Article
Language:English
Subjects:
Bayesian theory
Fourier transform infrared spectroscopy
Kinetics, Catalysis, and Reaction Engineering
methylamine
pesticides
synthesis
system optimization
temperature
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