Influence of powder/liquid mixing ratio on the performance of a restorative glass-ionomer dental cement

• Published in: Biomaterials 2003-10, Vol.24 (23), p.4173-4179
• Main Authors: Fleming, Garry J.P., Farooq, Ahmed A., Barralet, Jake E.
• Format: Article
• Language: English
• Subjects: Biocompatible Materials - chemistry; Compressive Strength; Dental Cements - chemistry; Glass Ionomer Cements - chemistry; Glass-ionomer dental cement; Image Processing, Computer-Assisted; Microscopy, Electron, Scanning; Mixing ratio; Oscillometry; Powders; Stress, Mechanical; Tensile Strength; Weibull statistics
• ISSN: 0142-9612; 1878-5905
• DOI: 10.1016/S0142-9612(03)00301-6

The influence of powder/liquid mixing regime on the performance of a hand-mixed restorative glass-ionomer cement (GIC) was evaluated in terms of compressive strength, working characteristics and the porosity distribution. Mean compressive fracture strengths, standard deviations and associated Weibull moduli ( m) were determined from series of 20 cylindrical specimens (6 mm height, 4 mm diameter) prepared by hand-mixing the relative proportions of the powder and liquid constituents. Working characteristics were assessed using an oscillating rheometer whilst scanning electron microscopy and image analysis were used to investigate the influence of the mixing regime on pore distribution. For a constant volume of liquid (1 ml) the mean compressive strength decreased from 102.1±23.1 MPa for 7.4 g of powder, to 93.8±22.9, 82.6±18.5 and 55.7±17.2 MPa for 6.66, 5.94 and 3.7 g of powder, respectively. A concomitant increase in both the working and setting times was also observed. GICs manipulated to a powder/liquid mixing consistency below the manufacturers’ recommend ratio, for a constant volume of liquid, resulted in reduced porosity levels in the cement mass and extended working and setting times. Unfortunately, a reduction in the concentration of reinforcing glass particles in the set material below that specified by the manufacturers decreases the cements’ load bearing capacity so that they fail at lower compressive stress levels in the posterior region of the mouth.