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Structure elucidation and complete NMR spectral assignment of an unusual aromatic monacolin analog from Monascus purpureus-fermented rice

One unusual aromatic monacolin analog, monacophenyl, was isolated from the ethanolic extract of Monascus purpureus‐fermented rice. Its structure was completely and unambiguously assigned by one‐ and two‐dimensional NMR techniques (1H NMR, 13C NMR, HSQC, HMBC and NOESY) and high‐resolution ESI‐MS spe...

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Published in:Magnetic resonance in chemistry 2011-03, Vol.49 (3), p.129-131
Main Authors: Liu, Ming-Tao, Li, Jin-Jie, Shang, Xiao-Ya, Li, Shuai, Li, Ling-Ling, Luan, Na, Jin, Zong-Lian
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cited_by cdi_FETCH-LOGICAL-c3914-ec403e970a8fa9d20f453da5a21a0d924650fd2bf77bda6e9a9e89d6f1cb26773
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container_title Magnetic resonance in chemistry
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creator Liu, Ming-Tao
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Jin, Zong-Lian
description One unusual aromatic monacolin analog, monacophenyl, was isolated from the ethanolic extract of Monascus purpureus‐fermented rice. Its structure was completely and unambiguously assigned by one‐ and two‐dimensional NMR techniques (1H NMR, 13C NMR, HSQC, HMBC and NOESY) and high‐resolution ESI‐MS spectrometry. Copyright © 2011 John Wiley & Sons, Ltd. One unusual aromatic monacolin analog, monacophenyl, was isolated from the ethanolic extract of Monascus purpureus‐fermented rice. Its structure was completely and unambiguously assigned by one‐ and two‐dimensional NMR techniques (1H NMR, 13C NMR, HSQC, HMBC and NOESY) and high‐resolution ESI‐MS spectrometry.
doi_str_mv 10.1002/mrc.2714
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source Wiley:Jisc Collections:Wiley Read and Publish Open Access 2024-2025 (reading list)
subjects 13C
2D NMR
Anticholesteremic Agents - chemistry
Lovastatin - analogs & derivatives
Lovastatin - chemistry
Magnetic Resonance Spectroscopy
Molecular Structure
monacolin analog
Monascus
Monascus - chemistry
Monascus purpureus-fermented rice
NMR
Oryza - chemistry
Oryza sativa
Pyrones - chemistry
Tetrahydronaphthalenes - chemistry
title Structure elucidation and complete NMR spectral assignment of an unusual aromatic monacolin analog from Monascus purpureus-fermented rice
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